Cuprosklodowskite Diffraction data computed using the structute from the paper listed below, along with the cell parameters refined from single crystal data of R060570 Rosenzweig A, Ryan R R American Mineralogist 60 (1975) 448-453 Refinement of the crystal structure of cuprosklodowskite, Cu[(UO2)2(SiO3OH)2]*6(H2O) CELL PARAMETERS: 7.0500 9.2400 6.6500 109.020 89.810 109.590 SPACE GROUP: P-1 ATOM X Y Z OCCUPANCY ISO(B) U 0.25890 0.21000 0.63970 1.000 0.586 Cu 0.50000 0.50000 0.00000 1.000 2.114 Si 0.77350 0.05260 0.85730 1.000 0.866 O 0.35300 0.23500 0.69900 1.000 1.271 O 0.83800 0.19300 0.41600 1.000 1.184 O 0.58800 0.02400 0.69200 1.000 0.897 O 0.93200 0.01800 0.69000 1.000 0.819 O 0.86300 0.24800 0.02100 1.000 1.753 O 0.72000 0.94000 0.00200 1.000 0.933 Wa 0.46500 0.37400 0.19300 1.000 2.945 Wa 0.23100 0.51300 0.05200 1.000 3.652 Wa 0.20100 0.48200 0.49900 1.000 4.310 X-RAY WAVELENGTH: 1.541838 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 6 +/- 7 +/- 5 MAX. ABS. INTENSITY / VOLUME**2: 65.83846376 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 10.83 7.79 8.1715 0 1 0 13.43 4.16 6.5948 1 0 0 13.96 100.00 6.3437 -1 1 0 14.19 10.15 6.2423 0 0 1 14.59 80.22 6.0721 0 -1 1 18.35 4.95 4.8351 1 -1 1 18.37 28.25 4.8293 -1 0 1 20.07 18.63 4.4242 1 1 0 20.67 8.63 4.2971 0 1 1 20.72 8.37 4.2861 1 0 1 21.15 2.62 4.2012 -1 2 0 21.30 20.49 4.1719 -1 -1 1 21.45 11.09 4.1433 -1 1 1 21.50 1.54 4.1333 0 -2 1 21.75 5.43 4.0858 0 2 0 21.96 50.41 4.0467 1 -2 1 25.30 12.77 3.5200 -2 1 0 26.83 6.40 3.3224 0 -1 2 27.04 22.10 3.2974 2 0 0 27.65 13.26 3.2267 1 1 1 28.13 8.53 3.1718 -2 2 0 28.51 17.89 3.1313 -1 -2 1 28.73 1.72 3.1072 -1 2 1 28.85 6.40 3.0947 2 -1 1 29.08 8.39 3.0703 -2 0 1 29.40 11.70 3.0382 -2 1 1 29.42 7.01 3.0360 0 -2 2 29.51 3.05 3.0270 1 2 0 29.91 5.73 2.9877 1 -1 2 29.98 23.96 2.9801 0 2 1 30.19 21.53 2.9606 -1 0 2 30.33 2.65 2.9469 -1 -1 2 30.55 4.00 2.9260 1 -2 2 30.77 5.93 2.9060 -1 3 0 30.96 10.79 2.8880 0 -3 1 32.17 3.50 2.7821 2 0 1 32.76 5.19 2.7341 -2 -1 1 32.88 6.76 2.7238 0 3 0 33.18 14.01 2.6997 1 0 2 33.60 8.52 2.6675 -2 2 1 34.10 17.40 2.6292 0 1 2 34.11 13.26 2.6288 2 -3 1 34.28 10.17 2.6157 -1 -2 2 34.51 8.72 2.5990 -2 3 0 34.93 13.80 2.5689 1 -3 2 35.49 10.82 2.5291 0 -3 2 36.80 8.34 2.4426 1 2 1 37.19 5.99 2.4175 2 -2 2 38.06 14.66 2.3646 -1 3 1 38.12 5.91 2.3607 2 -1 2 38.46 2.68 2.3405 -3 1 0 38.61 7.77 2.3317 2 1 1 38.81 4.74 2.3206 -2 -1 2 38.98 5.08 2.3108 -2 1 2 39.00 4.58 2.3094 1 -4 1 39.07 5.08 2.3056 -3 2 0 39.42 1.07 2.2856 -2 -2 1 39.56 2.59 2.2780 2 -3 2 40.03 4.29 2.2522 1 3 0 40.53 6.96 2.2260 -1 2 2 40.76 4.73 2.2135 3 -2 1 40.79 5.55 2.2121 2 2 0 40.80 8.49 2.2119 -3 1 1 41.08 5.40 2.1972 -1 -3 2 41.35 4.10 2.1834 0 -2 3 41.35 1.28 2.1833 2 -4 1 41.39 4.94 2.1815 -1 4 0 41.92 1.60 2.1553 -3 0 1 42.76 4.04 2.1146 -3 3 0 42.82 4.31 2.1121 -1 -1 3 43.06 1.21 2.1006 -2 4 0 43.49 5.99 2.0808 0 0 3 43.65 7.07 2.0734 1 -1 3 43.80 2.27 2.0667 0 -4 2 44.05 1.73 2.0558 -1 0 3 44.34 4.85 2.0429 0 4 0 44.78 1.15 2.0240 0 -3 3 44.79 5.30 2.0233 2 -4 2 44.87 1.84 2.0200 1 -3 3 45.34 4.80 2.0002 3 0 1 45.92 1.25 1.9761 -3 -1 1 46.41 6.28 1.9564 3 1 0 47.10 3.08 1.9295 2 2 1 47.15 2.95 1.9276 1 3 1 47.46 2.44 1.9156 -3 3 1 47.68 8.03 1.9072 -3 0 2 47.91 1.62 1.8986 1 2 2 47.97 3.46 1.8964 3 -4 1 48.06 4.31 1.8931 -2 -3 1 48.06 1.78 1.8931 -1 1 3 48.14 1.18 1.8903 3 -3 2 48.23 4.24 1.8868 -1 -4 1 48.51 4.87 1.8767 2 -2 3 48.70 2.36 1.8699 2 1 2 48.74 1.44 1.8683 0 1 3 48.90 1.73 1.8625 -2 0 3 48.98 4.07 1.8598 -1 -3 3 48.98 2.07 1.8598 -3 4 0 49.31 2.66 1.8479 3 -1 2 49.49 3.21 1.8418 -2 4 1 49.57 1.41 1.8391 1 -5 1 49.62 1.44 1.8373 1 -4 3 50.30 1.40 1.8140 -2 -3 2 50.38 1.37 1.8113 2 -5 1 50.44 1.02 1.8093 2 3 0 50.70 4.15 1.8008 0 -4 3 50.72 3.45 1.7999 -2 3 2 50.91 1.71 1.7936 1 -5 2 51.28 2.24 1.7815 1 4 0 51.50 2.12 1.7746 -2 1 3 51.65 1.57 1.7696 0 4 1 51.67 6.25 1.7690 -2 -2 3 52.30 2.42 1.7491 -3 -2 1 52.79 5.04 1.7343 0 -5 1 53.02 2.81 1.7273 -2 5 0 53.42 1.36 1.7151 1 1 3 53.79 2.02 1.7043 3 0 2 53.87 2.38 1.7019 -4 3 0 54.39 2.37 1.6870 -1 2 3 54.47 4.52 1.6845 -4 2 1 54.56 2.27 1.6820 4 -3 1 54.91 1.22 1.6722 2 0 3 55.06 1.20 1.6679 -3 -2 2 55.30 1.61 1.6612 0 -2 4 55.57 2.46 1.6537 4 -1 1 55.76 3.35 1.6487 4 0 0 56.05 2.16 1.6406 0 -1 4 56.15 1.73 1.6380 -3 3 2 56.29 1.89 1.6343 0 5 0 56.49 1.26 1.6291 -2 2 3 56.53 2.39 1.6279 1 -5 3 56.93 2.22 1.6174 1 -2 4 57.01 1.03 1.6154 0 -3 4 57.12 1.78 1.6127 -1 -1 4 57.15 2.29 1.6117 3 -3 3 57.29 3.06 1.6081 3 -5 2 57.55 1.15 1.6014 1 -3 4 58.21 1.39 1.5850 2 -5 3 58.34 2.53 1.5818 -3 -1 3 59.00 2.16 1.5657 -2 -4 2 59.21 1.06 1.5606 0 0 4 59.46 2.10 1.5545 -4 1 2 59.50 1.48 1.5536 -2 4 2 59.76 2.00 1.5474 4 -2 2 59.86 2.21 1.5450 -1 -5 2 59.89 1.96 1.5444 -1 5 1 60.29 1.15 1.5351 -4 -1 1 60.34 1.57 1.5340 3 -1 3 60.54 1.80 1.5293 1 -4 4 60.72 2.28 1.5254 2 -6 1 61.02 1.23 1.5184 1 -6 1 61.30 1.28 1.5123 2 -6 2 61.38 1.31 1.5104 4 -4 2 61.40 2.36 1.5101 1 2 3 61.72 1.60 1.5030 2 -3 4 62.03 1.26 1.4962 -3 -3 2 62.14 2.07 1.4937 -3 2 3 62.31 1.55 1.4900 0 4 2 62.77 2.25 1.4803 -2 0 4 63.08 1.93 1.4737 -3 5 1 63.45 1.57 1.4661 -3 4 2 63.51 1.56 1.4649 -2 3 3 63.54 1.48 1.4643 -1 1 4 64.10 1.07 1.4527 -1 -5 3 64.54 1.80 1.4440 0 -6 2 64.56 1.19 1.4435 -4 5 0 64.85 1.04 1.4378 0 -6 1 65.04 1.72 1.4340 -1 -4 4 65.12 1.25 1.4324 0 3 3 65.20 1.36 1.4309 1 -6 3 66.63 1.59 1.4035 -2 -3 4 66.80 1.76 1.4004 -3 6 0 66.98 1.72 1.3971 2 3 2 67.15 1.85 1.3939 0 -5 4 67.86 1.34 1.3812 -5 1 0 68.12 1.24 1.3764 2 4 1 68.36 1.81 1.3722 5 -2 1 68.79 1.14 1.3647 3 2 2 68.83 1.18 1.3641 1 4 2 68.93 1.15 1.3622 1 1 4 69.31 1.07 1.3557 -2 -5 1 69.66 1.04 1.3498 2 0 4 69.71 1.70 1.3489 3 -6 3 69.75 1.81 1.3482 -5 3 1 69.89 1.30 1.3459 -5 4 0 69.95 2.28 1.3450 3 -4 4 70.33 1.36 1.3386 -1 5 2 70.61 1.40 1.3339 1 5 1 70.62 1.61 1.3338 -4 4 2 71.45 1.09 1.3204 0 -3 5 71.75 2.05 1.3155 -3 1 4 71.81 1.21 1.3146 0 2 4 71.82 1.41 1.3144 4 -6 2 72.25 1.27 1.3077 3 1 3 72.38 1.60 1.3056 -1 -2 5 72.62 1.58 1.3019 1 -7 2 72.81 1.06 1.2989 1 -6 4 73.94 1.26 1.2819 4 2 1 74.13 1.07 1.2791 -1 -6 3 74.13 1.09 1.2790 4 1 2 74.30 1.20 1.2766 3 -7 1 75.02 1.01 1.2660 2 -7 3 75.35 1.35 1.2614 -4 3 3 76.30 1.07 1.2479 -2 7 0 76.81 1.46 1.2409 -2 -1 5 81.19 1.24 1.1847 2 -1 5 82.66 1.22 1.1674 0 7 0 82.69 1.15 1.1670 -2 5 3 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.