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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060287
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.014
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   53.5151 1.711324   2  1  1    2   53.5105  1.711461   -0.0046 -0.000137
   43.5497 2.077080   1  4  0    2   43.5467  2.077214   -0.0030 -0.000134
   58.7413 1.570873   0  6  0    2   58.7404  1.570895   -0.0009 -0.000022
   38.1758 2.356290   0  4  0    2   38.1749  2.356343   -0.0009 -0.000052
   50.2452 1.814787   0  4  1    2   50.2447  1.814803   -0.0005 -0.000017
   35.0809 2.556832   1  3  0    2   35.0806  2.556851   -0.0003 -0.000019
   68.1413 1.375220   0  6  1    2   68.1414  1.375219    0.0001  0.000001
   73.5041 1.287543   1  7  0    2   73.5043  1.287540    0.0002  0.000003
   62.7433 1.479932   1  5  1    2   62.7442  1.479913    0.0009  0.000019
   18.8271 4.712927   0  2  0    2   18.8281  4.712685    0.0010  0.000242
   38.8651 2.316057   1  1  1    2   38.8663  2.315985    0.0012  0.000071
   42.3924 2.131086   1  2  1    2   42.3939  2.131015    0.0015  0.000071
   60.8024 1.522452   2  3  1    2   60.8041  1.522414    0.0017  0.000038
   57.2545 1.608091   2  4  0    2   57.2563  1.608046    0.0018  0.000045
   27.7269 3.216320   1  2  0    2   27.7289  3.216092    0.0020  0.000228
   22.2892 3.987639   1  1  0    2   22.2935  3.986882    0.0043  0.000757

 rmse = 0.00002206543
 
     A =4.3999(2)              B =9.4254(1)               C =2.8453(1)           
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 117.996(4)