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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060760
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  0.710710
 Wavelength #2 =  0.709270
 Wavelength #3 =  0.713590
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.121
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    8.8597 4.654876   1  1  1    2    8.8718  4.648433    0.0121  0.006443
   11.3180 3.635161   1  3  1    2   11.3161  3.635791   -0.0019 -0.000630
   12.2644 3.352794   0  4  1    2   12.2829  3.347716    0.0185  0.005078
   12.5762 3.269180   2  2  1    2   12.5817  3.267742    0.0055  0.001437
   15.2699 2.690412   2  4  1    2   15.2451  2.694806   -0.0248 -0.004394
   17.0812 2.404860   3  3  1    2   17.0658  2.407025   -0.0154 -0.002165
   17.9980 2.282457   1  7  0    2   18.0005  2.282136    0.0025  0.000321
   19.8767 2.067260   3  1  2    2   19.9066  2.064171    0.0299  0.003090
   20.7510 1.980539   0  6  2    2   20.7176  1.983721   -0.0334 -0.003182
   23.3759 1.759563   3  5  2    2   23.3691  1.760067   -0.0068 -0.000504
   24.0181 1.712937   1  9  1    2   23.9882  1.715051   -0.0299 -0.002114
   25.3878 1.621469   2  4  3    2   25.4306  1.618771    0.0428  0.002698
   27.4896 1.499058   2 10  1    2   27.5234  1.497242    0.0338  0.001816
   28.6033 1.441584   6  2  1    2   28.6111  1.441199    0.0078  0.000385
   29.9923 1.375972   4  4  3    2   29.9595  1.377453   -0.0328 -0.001480
   34.6190 1.195970   2 12  2    2   34.6178  1.196012   -0.0012 -0.000042

 rmse = 0.00070322482
 
     A =9.084(7)               B =16.504(8)               C =5.727(5)            
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 858.6(7)