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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070418
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.026
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   20.0852 4.422825   0  2  0    2   20.0887  4.422068    0.0035  0.000757
   22.1234 4.019275   2  1  1    2   22.1204  4.019810   -0.0030 -0.000535
   26.9271 3.311477   1  2  1    2   26.9337  3.310678    0.0066  0.000799
   28.1019 3.175526   4  2  0    2   28.1005  3.175685   -0.0014 -0.000158
   30.3410 2.945887   3  2  1    2   30.3430  2.945698    0.0020  0.000189
   31.0861 2.876897   6  1  0    2   31.0865  2.876856    0.0004  0.000041
   31.6189 2.829585   5  1  1    2   31.6205  2.829444    0.0016  0.000140
   33.0652 2.708950   4  2  1    2   33.0632  2.709106   -0.0020 -0.000157
   35.3503 2.538771   1  3  1    2   35.3513  2.538698    0.0010  0.000072
   35.9597 2.497101   2  0  2    2   35.9617  2.496964    0.0020  0.000137
   36.2947 2.474802   5  2  1    2   36.2935  2.474883   -0.0012 -0.000081
   43.1085 2.097862   5  3  1    2   43.1053  2.098011   -0.0032 -0.000149
   46.3010 1.960290   6  3  1    2   46.2981  1.960406   -0.0029 -0.000116
   48.1605 1.888815   8  2  1    2   48.1615  1.888777    0.0010  0.000037
   51.0742 1.787635  10  1  0    2   51.0721  1.787705   -0.0021 -0.000070
   52.6880 1.736591   2  5  0    2   52.6904  1.736516    0.0024  0.000074
   53.7631 1.704356   8  3  1    2   53.7613  1.704408   -0.0018 -0.000052
   63.0364 1.473999   0  6  0    2   63.0353  1.474023   -0.0011 -0.000023
   67.1605 1.393119  11  3  1    2   67.1637  1.393060    0.0032  0.000059
   70.2064 1.339926   6  3  3    2   70.2058  1.339937   -0.0006 -0.000010

 rmse = 0.00002411276
 
     A =18.2539(4)             B =8.8441(2)               C =5.1920(2)           
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 838.20(3)