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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060189
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.041
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    9.7604 9.092697   0  2  0    2    9.7645  9.088906    0.0041  0.003792
   10.4664 8.478465   1  1  0    2   10.4711  8.474686    0.0047  0.003779
   18.1248 4.901413  -1  1  1    2   18.1316  4.899595    0.0068  0.001818
   19.5511 4.546187   0  4  0    2   19.5586  4.544453    0.0075  0.001734
   22.8434 3.896684  -1  3  1    2   22.8449  3.896427    0.0015  0.000257
   26.2327 3.399614   1  3  1    2   26.2404  3.398635    0.0077  0.000979
   27.0625 3.297069   2  4  0    2   27.0655  3.296713    0.0030  0.000356
   28.4071 3.143763   3  1  0    2   28.3958  3.144995   -0.0113 -0.001232
   32.5949 2.748267  -3  3  1    2   32.5872  2.748898   -0.0077 -0.000630
   32.9105 2.722597   1  5  1    2   32.9217  2.721695    0.0112  0.000901
   34.4008 2.607841   0  6  1    2   34.4000  2.607897   -0.0008 -0.000056
   35.2851 2.544407  -2  0  2    2   35.2917  2.543949    0.0066  0.000458
   38.2814 2.351649  -3  5  1    2   38.2743  2.352070   -0.0071 -0.000421
   39.4237 2.286030  -3  1  2    2   39.4206  2.286203   -0.0031 -0.000173
   44.1285 2.052371   2  0  2    2   44.1233  2.052602   -0.0052 -0.000231
   55.3268 1.660239   4  6  1    2   55.3280  1.660207    0.0012  0.000033
   56.5029 1.628415   1 11  0    2   56.5006  1.628475   -0.0023 -0.000061
   64.3348 1.447651  -6  6  1    2   64.3382  1.447583    0.0034  0.000068

 rmse = 0.00005175568
 
     A =9.9046(7)              B =18.178(1)               C =5.2980(6)           
 Alpha =90                  Beta =104.721(7)          Gamma =90                  
 
 Volume = 922.6(0)