Fizelyite Diffraction data computed using the structure determined in our lab for sample R060175 CELL PARAMETERS: 19.2779 13.2352 8.7235 90.000 90.402 90.000 SPACE GROUP: P2_1/n ATOM X Y Z OCCUPANCY ISO(B) Sb 0.34869 0.37360 0.14217 1.000 1.803 Pb 0.04886 0.61574 0.13065 1.000 2.195 Pb 0.25025 0.58261 0.40131 1.000 2.460 Ag 0.14177 0.32170 0.11580 0.961 4.478 Sb 0.44281 0.61815 0.12555 1.000 1.716 Sb 0.37224 0.35338 0.61916 1.000 1.683 Sb 0.44642 0.63072 0.63707 1.000 1.775 Pb 0.25337 0.59674 0.89487 1.000 2.536 Pb 0.12790 0.35108 0.61537 0.682 2.158 Ag 0.11352 0.35040 0.53231 0.262 7.251 Sb 0.05207 0.62499 0.64418 1.000 1.672 Ag 0.17351 0.38437 0.83743 0.198 3.132 S 0.09972 0.53124 0.43133 1.000 2.397 S 0.02004 0.25122 0.06867 1.000 2.046 S 0.23045 0.45369 0.14532 1.000 1.938 S 0.33640 0.71493 0.12605 1.000 1.946 S 0.39473 0.49554 0.33498 1.000 1.846 S 0.16594 0.74281 0.08809 1.000 1.785 S 0.39726 0.49720 0.93351 1.000 1.730 S 0.50035 0.27497 0.15216 1.000 2.503 S 0.25862 0.44016 0.63751 1.000 1.997 S 0.33124 0.70623 0.64878 1.000 2.088 S 0.08700 0.50943 0.84853 1.000 2.321 S 0.15784 0.73268 0.66858 1.000 1.881 X-RAY WAVELENGTHS: 1.540562 1.544390 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 17 +/- 12 +/- 8 MAX. ABS. INTENSITY / VOLUME**2: 85.92468878 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 8.10 / 8.12 2.83 / 1.42 10.9111 1 1 0 13.01 / 13.04 4.10 / 2.05 6.8003 1 1 1 14.14 / 14.17 7.84 / 3.92 6.2591 1 2 0 15.28 / 15.32 1.91 / 0.96 5.7947 2 1 1 15.32 / 15.35 1.87 / 0.93 5.7805 3 1 0 16.23 / 16.27 5.01 / 2.51 5.4556 2 2 0 17.44 / 17.49 1.51 / 0.75 5.0800 1 2 1 18.45 / 18.50 1.60 / 0.80 4.8047 3 1 1 19.21 / 19.25 1.82 / 0.91 4.6172 2 2 1 19.24 / 19.29 1.11 / 0.55 4.6100 3 2 0 21.43 / 21.49 2.72 / 1.36 4.1425 0 1 2 22.14 / 22.20 1.58 / 0.79 4.0115 2 3 0 22.41 / 22.47 1.29 / 0.65 3.9633 2 0 2 22.81 / 22.87 7.04 / 3.52 3.8958 4 2 0 23.05 / 23.11 1.08 / 0.54 3.8549 1 3 1 23.30 / 23.36 23.67 / 11.84 3.8151 -2 1 2 23.41 / 23.47 14.40 / 7.20 3.7967 2 1 2 24.89 / 24.95 1.75 / 0.88 3.5747 1 2 2 25.48 / 25.55 26.47 / 13.24 3.4923 -3 1 2 25.64 / 25.71 32.52 / 16.26 3.4712 3 1 2 26.49 / 26.56 2.35 / 1.18 3.3617 -3 3 1 26.74 / 26.81 100.00 / 50.00 3.3313 5 2 0 26.92 / 26.99 25.24 / 12.62 3.3088 0 4 0 27.32 / 27.39 9.05 / 4.53 3.2611 1 4 0 27.74 / 27.81 4.41 / 2.21 3.2129 6 0 0 28.07 / 28.14 3.05 / 1.53 3.1763 -3 2 2 28.21 / 28.29 1.12 / 0.56 3.1604 3 2 2 28.29 / 28.36 1.05 / 0.53 3.1519 -4 1 2 28.76 / 28.83 2.46 / 1.23 3.1017 0 3 2 29.11 / 29.19 12.43 / 6.21 3.0647 -1 3 2 29.16 / 29.23 9.42 / 4.71 3.0599 1 3 2 29.22 / 29.30 2.65 / 1.33 3.0537 -4 3 1 30.20 / 30.28 36.07 / 18.04 2.9569 -2 3 2 30.29 / 30.37 32.79 / 16.40 2.9483 2 3 2 30.31 / 30.39 1.31 / 0.65 2.9460 -6 1 1 30.91 / 30.99 12.73 / 6.36 2.8903 6 2 0 31.95 / 32.03 17.90 / 8.95 2.7988 -3 3 2 32.08 / 32.16 22.61 / 11.30 2.7879 3 3 2 33.64 / 33.72 1.44 / 0.72 2.6621 0 2 3 33.93 / 34.02 1.03 / 0.52 2.6397 5 2 2 34.33 / 34.41 1.82 / 0.91 2.6103 1 4 2 35.23 / 35.32 1.24 / 0.62 2.5455 -2 4 2 35.27 / 35.36 1.49 / 0.74 2.5425 7 2 0 35.73 / 35.82 1.02 / 0.51 2.5107 1 5 1 37.28 / 37.38 1.42 / 0.71 2.4097 8 0 0 39.04 / 39.15 2.61 / 1.31 2.3050 6 4 0 39.13 / 39.23 8.88 / 4.44 2.3005 -7 1 2 39.38 / 39.48 6.04 / 3.02 2.2864 7 1 2 40.07 / 40.17 1.14 / 0.57 2.2484 -1 5 2 40.90 / 41.00 1.51 / 0.76 2.2048 -2 5 2 41.37 / 41.47 21.31 / 10.66 2.1808 0 0 4 41.95 / 42.06 1.31 / 0.65 2.1518 0 1 4 41.98 / 42.09 1.84 / 0.92 2.1503 2 6 0 42.19 / 42.30 1.22 / 0.61 2.1402 -1 1 4 42.26 / 42.37 9.98 / 4.99 2.1369 -3 5 2 42.36 / 42.47 10.63 / 5.31 2.1320 3 5 2 42.68 / 42.79 2.52 / 1.26 2.1167 7 4 0 43.28 / 43.39 12.18 / 6.09 2.0890 -8 1 2 43.32 / 43.43 1.11 / 0.56 2.0870 2 6 1 43.54 / 43.65 13.93 / 6.96 2.0769 8 1 2 43.96 / 44.08 1.05 / 0.52 2.0579 1 2 4 44.11 / 44.23 7.08 / 3.54 2.0512 -4 5 2 44.24 / 44.36 7.09 / 3.54 2.0455 4 5 2 45.15 / 45.27 1.36 / 0.68 2.0065 -7 0 3 45.17 / 45.29 8.37 / 4.18 2.0057 4 6 0 47.10 / 47.23 7.41 / 3.70 1.9277 10 0 0 47.45 / 47.57 10.88 / 5.44 1.9146 5 6 0 47.63 / 47.76 7.00 / 3.50 1.9075 -8 3 2 47.88 / 48.01 7.20 / 3.60 1.8983 8 3 2 49.12 / 49.25 2.67 / 1.34 1.8533 -6 5 2 49.30 / 49.43 1.81 / 0.91 1.8469 6 5 2 49.79 / 49.93 13.04 / 6.52 1.8297 -5 2 4 50.05 / 50.18 8.27 / 4.14 1.8209 0 4 4 50.09 / 50.22 11.43 / 5.72 1.8196 5 2 4 50.26 / 50.39 1.05 / 0.53 1.8138 -1 4 4 50.73 / 50.87 1.82 / 0.91 1.7981 9 4 0 52.18 / 52.32 2.35 / 1.18 1.7515 -7 5 2 52.35 / 52.49 1.05 / 0.52 1.7462 -6 2 4 52.38 / 52.52 2.10 / 1.05 1.7453 7 5 2 52.69 / 52.84 1.08 / 0.54 1.7356 6 2 4 52.94 / 53.08 1.52 / 0.76 1.7282 -1 7 2 52.97 / 53.11 1.54 / 0.77 1.7273 1 7 2 53.61 / 53.75 2.23 / 1.12 1.7082 -2 7 2 53.66 / 53.81 1.77 / 0.88 1.7065 2 7 2 54.09 / 54.23 2.80 / 1.40 1.6941 11 2 0 55.09 / 55.24 6.82 / 3.41 1.6657 10 4 0 55.50 / 55.65 1.72 / 0.86 1.6544 0 8 0 55.56 / 55.71 1.13 / 0.57 1.6526 -8 5 2 55.72 / 55.87 2.97 / 1.48 1.6483 1 8 0 56.38 / 56.53 1.94 / 0.97 1.6306 2 8 0 62.80 / 62.97 1.69 / 0.85 1.4785 -4 6 4 63.00 / 63.18 1.44 / 0.72 1.4742 4 6 4 64.21 / 64.39 2.28 / 1.14 1.4494 -10 0 4 64.61 / 64.79 2.88 / 1.44 1.4413 -5 6 4 64.71 / 64.89 2.14 / 1.07 1.4393 10 0 4 64.86 / 65.04 3.07 / 1.54 1.4363 5 6 4 65.15 / 65.33 1.03 / 0.51 1.4307 -2 1 6 65.22 / 65.40 1.88 / 0.94 1.4294 -12 3 2 65.52 / 65.70 1.34 / 0.67 1.4236 12 3 2 66.34 / 66.53 1.60 / 0.80 1.4079 3 1 6 66.44 / 66.63 1.07 / 0.54 1.4060 8 7 2 66.81 / 67.00 2.58 / 1.29 1.3991 -13 1 2 67.13 / 67.32 2.49 / 1.25 1.3932 13 1 2 68.53 / 68.72 1.43 / 0.72 1.3682 -2 3 6 69.69 / 69.89 1.04 / 0.52 1.3482 3 3 6 70.21 / 70.41 1.07 / 0.53 1.3395 -4 9 2 70.30 / 70.51 1.01 / 0.51 1.3379 4 9 2 70.93 / 71.13 2.16 / 1.08 1.3276 -10 4 4 71.41 / 71.61 1.90 / 0.95 1.3199 10 4 4 72.07 / 72.28 1.05 / 0.52 1.3093 9 8 0 75.26 / 75.48 1.49 / 0.75 1.2616 15 2 0 76.48 / 76.70 1.04 / 0.52 1.2445 -7 9 2 77.13 / 77.36 1.23 / 0.62 1.2356 8 1 6 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.