Gelosaite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from single crystal data of R120031 Orlandi P, Demartin F, Pasero M, Leverett P, Williams P A, Hibbs D E American Mineralogist 96 (2011) 268-273 Gelosaite, BiMo6+(2-5x)Mo5+6xO7(OH)*H2O (0<=x<=0.4), a new mineral from Su Senargiu (CA), Sardinia, Italy, and a second occurrence from Kingsgate, New England, Australia Locality: Su Senargiu, Sardinia, Italy _database_code_amcsd 0018668 CELL PARAMETERS: 5.8540 9.0480 13.9140 90.000 100.410 90.000 SPACE GROUP: P2_1/n ATOM X Y Z OCCUPANCY ISO(B) Bi 0.40357 0.41689 0.10649 1.000 0.791 Mo 0.86623 0.10399 0.15719 1.000 0.711 Mo 0.63232 0.22137 0.34084 1.000 0.732 Mo 0.63210 -0.04430 0.33960 0.028 0.979 Mo 1.09370 0.25970 0.39430 0.074 1.611 Ow 0.96060 0.41720 0.34252 1.000 1.571 O 0.75480 0.09301 0.03404 1.000 1.255 O 0.39990 0.10589 0.33664 1.000 1.453 O 0.63970 0.24002 0.19069 1.000 1.019 O 0.74500 0.24350 0.46385 1.000 1.413 Oh 0.82310 -0.08846 0.48180 1.000 1.003 O 1.01210 -0.08756 0.18310 1.000 0.924 O 0.86490 0.08618 0.31149 1.000 0.900 O 1.10090 0.21738 0.16456 1.000 1.595 H 1.02800 0.42600 0.30300 1.000 3.790 H 1.04100 0.42800 0.39300 1.000 2.685 H 0.75780 -0.16960 0.48940 1.000 3.948 X-RAY WAVELENGTH: 1.541838 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 5 +/- 8 +/- 12 MAX. ABS. INTENSITY / VOLUME**2: 48.46027243 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 11.73 75.44 7.5475 0 1 1 12.94 6.53 6.8425 0 0 2 15.58 38.83 5.6871 -1 0 1 16.24 9.67 5.4576 0 1 2 18.26 100.00 4.8575 1 1 0 18.43 42.55 4.8149 -1 1 1 20.75 30.66 4.2809 -1 1 2 23.58 3.78 3.7738 0 2 2 24.03 37.11 3.7034 1 1 2 25.03 50.53 3.5573 1 2 0 26.04 59.40 3.4212 0 0 4 26.59 32.32 3.3529 1 2 1 26.93 52.18 3.3111 -1 2 2 27.04 10.68 3.2972 1 0 3 27.77 19.32 3.2122 0 2 3 27.88 5.15 3.2001 0 1 4 28.82 12.97 3.0979 1 1 3 29.56 21.86 3.0224 -1 1 4 29.57 53.90 3.0212 1 2 2 30.08 14.94 2.9706 -1 2 3 31.46 43.74 2.8435 -2 0 2 32.44 62.96 2.7598 0 3 2 32.82 1.45 2.7288 0 2 4 33.02 2.17 2.7127 -2 1 2 33.62 22.70 2.6657 -1 0 5 34.23 18.37 2.6198 0 1 5 34.28 11.32 2.6161 -1 2 4 34.28 7.63 2.6157 1 1 4 34.43 4.05 2.6048 2 1 1 35.09 3.71 2.5571 -1 1 5 35.15 11.43 2.5531 -2 1 3 35.96 19.87 2.4971 2 0 2 36.58 8.81 2.4567 -2 2 1 37.00 2.59 2.4296 -2 0 4 37.01 1.63 2.4288 2 2 0 37.56 13.46 2.3946 -1 3 3 38.44 3.01 2.3418 0 2 5 38.49 10.00 2.3389 1 2 4 38.90 3.17 2.3150 1 0 5 39.28 2.32 2.2938 -2 2 3 39.51 4.23 2.2808 0 0 6 39.85 2.22 2.2624 0 3 4 39.85 2.91 2.2620 0 4 0 40.42 7.43 2.2317 0 4 1 40.54 4.45 2.2254 1 3 3 40.80 1.48 2.2116 0 1 6 41.22 6.01 2.1903 2 1 3 42.22 3.76 2.1405 -2 2 4 42.45 2.86 2.1296 -2 1 5 42.96 2.66 2.1054 1 4 0 43.46 52.18 2.0824 2 3 0 43.93 3.57 2.0609 1 2 5 43.94 2.42 2.0605 1 4 1 44.16 6.37 2.0507 -1 4 2 44.48 3.98 2.0366 0 2 6 44.65 1.23 2.0295 2 0 4 44.72 7.05 2.0265 0 4 3 44.74 5.75 2.0255 -1 2 6 45.41 1.90 1.9974 -1 3 5 45.82 2.25 1.9803 2 1 4 45.93 2.84 1.9759 1 4 2 46.02 11.27 1.9720 -2 2 5 46.09 4.15 1.9693 -2 0 6 46.27 2.54 1.9623 -1 0 7 46.49 5.75 1.9532 1 1 6 47.24 3.74 1.9243 -2 1 6 47.26 1.63 1.9234 2 3 2 47.93 9.03 1.8982 -3 1 2 47.99 11.04 1.8957 -3 0 3 48.09 15.77 1.8921 -2 3 4 48.23 2.01 1.8869 0 4 4 48.49 2.42 1.8774 3 1 0 49.10 1.85 1.8554 -3 1 3 49.64 10.51 1.8364 1 3 5 49.84 5.31 1.8295 1 2 6 50.15 7.86 1.8192 0 3 6 50.20 2.93 1.8173 3 1 1 50.88 12.81 1.7946 0 2 7 51.01 3.13 1.7905 -3 2 1 51.04 6.32 1.7895 -2 4 1 51.20 2.98 1.7840 -3 2 2 51.63 1.56 1.7702 -2 4 2 51.74 8.42 1.7668 3 2 0 52.05 11.04 1.7571 1 0 7 52.52 4.95 1.7424 1 4 4 52.60 7.28 1.7400 -2 1 7 52.79 6.25 1.7340 3 1 2 53.05 10.62 1.7263 1 5 0 53.11 4.22 1.7244 -1 5 1 54.05 1.65 1.6966 -1 1 8 54.08 7.96 1.6958 -1 5 2 54.17 3.59 1.6930 2 2 5 54.33 3.30 1.6885 -3 2 4 54.50 18.86 1.6838 2 3 4 54.60 1.93 1.6808 0 1 8 54.75 1.17 1.6765 2 4 2 55.61 6.25 1.6528 1 5 2 55.68 2.71 1.6508 -2 2 7 55.76 5.56 1.6486 2 0 6 55.87 2.63 1.6457 3 2 2 55.90 17.58 1.6448 -1 3 7 56.18 7.02 1.6374 -3 3 1 57.58 4.81 1.6006 -1 4 6 57.69 2.72 1.5978 2 4 3 57.83 2.24 1.5944 -3 1 6 58.15 2.53 1.5864 1 5 3 58.57 2.49 1.5760 -1 5 4 58.66 3.88 1.5738 -2 4 5 59.13 2.00 1.5623 3 2 3 60.06 8.83 1.5405 -1 0 9 60.12 1.55 1.5390 -2 5 1 60.28 1.27 1.5354 3 1 4 61.03 1.31 1.5182 1 3 7 61.26 7.27 1.5130 -3 0 7 61.35 2.05 1.5112 -2 2 8 61.42 4.10 1.5095 0 5 5 61.46 5.03 1.5087 1 5 4 61.49 8.59 1.5080 0 6 0 61.88 5.19 1.4995 0 1 9 61.98 10.77 1.4972 -3 3 5 62.02 2.17 1.4964 -2 5 3 62.83 2.11 1.4791 0 4 7 62.95 4.28 1.4765 2 1 7 63.11 5.32 1.4731 3 2 4 63.58 2.24 1.4634 3 4 0 63.86 1.16 1.4576 -1 6 1 64.41 1.73 1.4466 2 3 6 64.71 3.12 1.4406 -4 1 1 64.77 5.03 1.4394 4 0 0 64.78 1.44 1.4391 -2 1 9 65.02 1.01 1.4344 3 1 5 65.67 1.21 1.4218 -4 0 4 65.73 1.45 1.4207 2 4 5 65.87 2.71 1.4180 -3 4 4 66.08 1.24 1.4139 -1 5 6 66.36 1.34 1.4087 1 0 9 67.08 3.10 1.3953 -2 5 5 67.27 1.26 1.3919 -4 2 2 67.44 1.95 1.3888 -4 2 1 67.51 4.13 1.3874 -2 2 9 67.88 2.20 1.3808 -4 2 3 67.93 4.62 1.3799 0 6 4 68.38 1.44 1.3719 -1 3 9 68.77 1.60 1.3651 -4 1 5 70.36 2.12 1.3381 3 1 6 70.70 1.54 1.3325 -2 5 6 70.71 4.77 1.3322 -2 6 2 70.97 1.01 1.3280 0 5 7 71.24 3.37 1.3237 -3 5 2 71.42 3.13 1.3207 -4 2 5 71.68 2.18 1.3166 3 5 0 71.71 3.29 1.3162 -4 3 2 71.94 2.77 1.3125 -1 6 5 72.11 1.19 1.3099 0 2 10 73.05 1.39 1.2954 3 5 1 73.19 1.01 1.2932 4 1 3 73.34 3.52 1.2909 2 6 2 73.61 1.65 1.2868 0 7 1 73.62 1.69 1.2867 1 4 8 74.30 1.51 1.2765 -4 2 6 74.32 5.65 1.2763 1 3 9 74.90 1.13 1.2677 1 1 10 74.99 4.91 1.2665 -2 5 7 75.15 4.73 1.2642 3 5 2 75.20 1.15 1.2636 1 6 5 75.32 1.02 1.2618 -4 1 7 76.26 3.68 1.2486 4 0 4 76.56 1.69 1.2445 2 3 8 76.65 1.10 1.2431 0 5 8 76.90 5.34 1.2397 4 3 2 77.88 2.89 1.2265 -4 2 7 78.33 1.16 1.2207 -4 4 3 78.81 1.45 1.2144 -2 1 11 79.26 3.08 1.2086 2 2 9 79.65 4.66 1.2038 -3 3 9 79.98 3.40 1.1996 0 2 11 80.04 1.51 1.1988 -1 7 4 80.16 1.02 1.1973 -2 6 6 80.45 1.34 1.1937 4 4 1 81.28 1.33 1.1837 -1 4 10 81.57 2.55 1.1801 -3 6 3 82.17 1.74 1.1731 1 0 11 82.65 1.72 1.1674 2 7 1 82.79 4.68 1.1658 -1 3 11 82.85 1.38 1.1652 -5 0 1 82.94 4.00 1.1641 0 5 9 83.04 2.18 1.1630 3 3 7 83.07 1.06 1.1627 -2 7 3 83.90 3.15 1.1532 2 5 7 84.70 2.62 1.1443 1 6 7 84.88 2.29 1.1424 -3 0 11 84.89 1.32 1.1423 5 1 0 85.29 1.04 1.1380 3 2 8 85.34 2.94 1.1374 -5 0 5 85.72 1.04 1.1334 -5 2 2 85.89 1.30 1.1315 -4 5 3 87.71 2.22 1.1127 2 6 6 88.00 1.88 1.1098 1 8 0 88.83 1.72 1.1016 -1 8 2 89.08 1.18 1.0991 3 0 9 89.22 1.20 1.0978 -4 5 5 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.