Giniite Note: R060765 Locality: Sandamab, Namibia CELL PARAMETERS: 10.3472 5.1497 14.2338 90.000 111.175 90.000 SPACE GROUP: P2/n ATOM X Y Z OCCUPANCY ISO(B) Fe 0.75000 1.21895 0.75000 1.000 0.481 Fe 0.75559 0.48900 0.51184 1.000 0.501 Fe 0.97559 -0.24626 0.25478 1.000 0.786 P 0.55669 0.72162 0.62842 1.000 0.348 P 0.93837 0.24450 0.37905 1.000 0.441 O 0.80559 1.23366 0.62758 1.000 0.599 O 0.40011 0.73247 0.57251 1.000 0.739 O 0.59413 0.47645 0.69647 1.000 0.666 O 0.63708 0.71581 0.55788 1.000 0.760 O 1.09551 0.26866 0.41789 1.000 0.810 O 0.80215 -0.21698 0.11120 1.000 0.703 O 0.59568 0.96362 0.69697 1.000 0.672 O 0.87463 0.30045 0.45728 1.000 0.876 O 0.87708 0.43833 0.28937 1.000 0.918 O 0.89752 -0.03074 0.33717 1.000 0.847 H 0.82775 -0.05243 0.09286 1.000 1.980 H 0.71984 -0.16970 0.12268 1.000 4.219 H 0.80661 1.06191 0.60168 1.000 1.516 X-RAY WAVELENGTH: 1.541838 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 8 +/- 4 +/- 12 Cell Volume: 707.238 Density (g/cm3): 3.424 MAX. ABS. INTENSITY / VOLUME**2: 14.94876185 RIR: 1.422 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.18 7.44 9.6328 -1 0 1 2 13.15 10.32 6.7329 1 0 1 2 13.34 8.88 6.6364 0 0 2 2 17.22 20.69 5.1497 0 1 0 2 18.42 7.32 4.8164 -2 0 2 2 18.48 13.07 4.8010 0 1 1 4 18.80 1.05 4.7190 -1 0 3 2 19.54 5.42 4.5431 1 1 0 4 21.75 1.29 4.0868 -1 1 2 4 21.85 29.42 4.0685 0 1 2 4 24.39 1.85 3.6498 -2 1 1 4 25.30 10.07 3.5207 2 1 0 4 25.32 14.73 3.5176 -2 1 2 4 25.58 2.67 3.4829 1 1 2 4 25.60 1.31 3.4791 -1 1 3 4 26.04 4.49 3.4214 -3 0 1 2 26.48 46.59 3.3665 2 0 2 2 26.54 27.23 3.3584 -2 0 4 2 26.56 100.00 3.3558 0 1 3 4 26.87 4.62 3.3182 0 0 4 2 27.78 1.37 3.2109 -3 0 3 2 27.88 21.66 3.2004 2 1 1 4 27.92 49.56 3.1958 -2 1 3 4 30.51 5.59 2.9303 1 1 3 4 30.54 1.13 2.9272 -1 1 4 4 30.88 4.59 2.8955 3 0 1 2 31.40 8.70 2.8485 -3 1 2 4 31.56 1.80 2.8347 -1 0 5 2 31.76 9.66 2.8178 2 1 2 4 31.81 7.10 2.8131 -2 1 4 4 32.09 12.46 2.7893 0 1 4 4 32.83 6.41 2.7279 3 1 0 4 34.68 6.16 2.5868 -4 0 2 2 34.84 13.47 2.5749 0 2 0 2 35.22 3.73 2.5485 -3 0 5 2 35.51 3.09 2.5277 0 2 1 4 35.63 6.47 2.5197 -3 1 4 4 36.13 3.28 2.4858 1 1 4 4 36.57 6.06 2.4573 2 1 3 4 36.63 3.32 2.4531 -2 1 5 4 37.28 1.14 2.4121 4 0 0 2 37.34 3.24 2.4082 -4 0 4 2 37.46 5.72 2.4005 0 2 2 4 38.14 4.58 2.3595 0 1 5 4 38.96 3.76 2.3115 -4 1 2 4 39.37 4.32 2.2885 3 1 2 4 39.56 12.72 2.2781 -4 1 1 4 39.59 3.80 2.2764 -4 1 3 4 39.68 12.75 2.2716 2 2 0 4 40.79 1.79 2.2121 0 0 6 2 41.33 1.73 2.1844 4 1 0 4 41.39 1.35 2.1815 -4 1 4 4 42.05 4.19 2.1485 2 1 4 4 42.13 2.55 2.1450 -2 1 6 4 43.36 1.56 2.0870 1 2 3 4 44.01 4.37 2.0573 -3 2 1 4 44.11 2.50 2.0533 -3 1 6 4 44.17 10.22 2.0506 4 1 1 4 44.25 12.50 2.0470 -4 1 5 4 44.29 3.32 2.0452 2 2 2 4 44.33 9.22 2.0434 -2 2 4 4 44.35 6.06 2.0425 4 0 2 2 44.46 3.00 2.0377 -4 0 6 2 44.54 3.72 2.0342 0 2 4 4 44.58 1.67 2.0325 0 1 6 4 45.14 4.35 2.0088 -3 2 3 4 45.95 1.58 1.9751 -3 0 7 2 47.24 1.39 1.9241 3 2 1 4 47.91 3.66 1.8986 4 1 2 4 48.02 4.75 1.8948 -4 1 6 4 48.06 4.89 1.8932 2 1 5 4 48.14 3.45 1.8903 -2 1 7 4 48.80 1.92 1.8663 -1 1 7 4 49.98 12.84 1.8249 -4 2 2 4 50.31 1.20 1.8135 3 2 2 4 50.38 1.51 1.8113 -3 2 5 4 51.28 3.22 1.7817 2 0 6 2 51.35 3.43 1.7793 0 1 7 4 51.99 2.11 1.7590 3 0 5 2 53.85 1.09 1.7024 0 3 1 4 54.22 2.74 1.6918 3 2 3 4 54.50 2.67 1.6838 2 1 6 4 54.52 5.69 1.6832 4 0 4 2 54.58 1.55 1.6814 -2 1 8 4 54.66 8.61 1.6792 -4 0 8 2 54.70 17.89 1.6779 0 2 6 4 55.29 2.41 1.6614 -3 1 8 4 55.38 4.47 1.6591 0 0 8 2 56.70 1.44 1.6235 -6 1 2 4 56.74 1.23 1.6225 -6 1 4 4 56.94 3.44 1.6172 2 3 0 4 56.95 1.95 1.6169 -2 3 2 4 57.29 3.29 1.6081 6 0 0 2 57.39 3.01 1.6055 -6 0 6 2 57.60 9.68 1.6003 0 3 3 4 57.60 21.69 1.6002 4 2 2 4 57.69 12.69 1.5979 -4 2 6 4 58.06 2.84 1.5886 -6 1 1 4 58.13 3.10 1.5869 -6 1 5 4 58.33 3.85 1.5820 -2 3 3 4 58.69 2.88 1.5730 -3 0 9 2 58.94 3.10 1.5671 -3 2 7 4 60.33 1.42 1.5341 -3 3 2 4 60.39 1.87 1.5327 -6 1 6 4 60.75 2.18 1.5246 0 3 4 4 62.97 1.59 1.4761 -7 0 3 2 63.38 4.76 1.4676 4 1 5 4 63.53 1.83 1.4644 -4 1 9 4 63.57 5.24 1.4636 -2 2 8 4 63.87 2.27 1.4574 -7 0 5 2 64.51 1.38 1.4446 1 2 7 4 64.66 1.60 1.4414 0 3 5 4 65.51 1.04 1.4249 -6 2 2 4 65.51 1.26 1.4248 3 3 2 4 65.64 1.80 1.4223 -4 3 1 4 65.84 1.27 1.4186 -7 1 4 4 65.88 1.36 1.4178 0 1 9 4 66.64 1.39 1.4033 -7 1 2 4 66.90 2.45 1.3986 4 3 0 4 66.94 1.60 1.3978 -4 3 4 4 67.11 2.68 1.3946 0 2 8 4 67.16 1.12 1.3937 6 1 2 4 68.39 1.16 1.3717 -7 1 6 4 68.49 1.64 1.3700 -3 1 10 4 70.76 1.59 1.3315 7 1 0 4 71.69 1.73 1.3164 6 1 3 4 71.95 2.05 1.3123 2 3 5 4 72.01 1.40 1.3114 -2 3 7 4 73.17 5.57 1.2934 -8 0 4 2 73.57 5.90 1.2874 0 4 0 2 74.14 1.75 1.2789 -7 1 8 4 76.40 2.43 1.2467 -2 1 11 4 76.55 1.87 1.2445 4 1 7 4 76.73 1.81 1.2421 -4 1 11 4 77.23 1.60 1.2353 -2 3 8 4 78.87 1.03 1.2137 -7 2 7 4 79.34 1.04 1.2076 -8 1 1 4 79.46 1.24 1.2061 -8 1 7 4 79.75 1.96 1.2025 2 4 2 4 80.19 1.02 1.1970 -6 3 1 4 81.41 2.08 1.1821 4 0 8 2 81.61 2.63 1.1798 0 2 10 4 81.61 1.09 1.1797 -4 0 12 2 84.71 1.76 1.1443 6 2 4 4 84.86 1.15 1.1426 4 3 5 4 89.95 1.50 1.0907 -8 2 8 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.