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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070124
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.014
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    9.7263 9.099107   0  2  0    2    9.7321  9.093646    0.0058  0.005461
   10.4326 8.483791   1  1  0    2   10.4366  8.480539    0.0040  0.003252
   17.3037 5.124634   1  3  0    2   17.3064  5.123837    0.0027  0.000797
   18.5121 4.792498   2  0  0    2   18.5091  4.793257   -0.0030 -0.000758
   19.5183 4.547471   0  4  0    2   19.5211  4.546823    0.0028  0.000648
   26.1641 3.404898   1  3  1    2   26.1680  3.404402    0.0039  0.000496
   27.0209 3.298790   2  4  0    2   27.0211  3.298770    0.0002  0.000020
   28.3589 3.146041   3  1  0    2   28.3474  3.147294   -0.0115 -0.001254
   30.2105 2.957214   2  2  1    2   30.2014  2.958081   -0.0091 -0.000866
   32.4512 2.757868  -3  3  1    2   32.4463  2.758275   -0.0049 -0.000406
   32.8431 2.725836   1  5  1    2   32.8514  2.725165    0.0083  0.000671
   34.3088 2.612618   0  6  1    2   34.3148  2.612176    0.0060  0.000442
   38.1363 2.358648  -3  5  1    2   38.1427  2.358267    0.0064  0.000382
   40.4091 2.231028  -2  4  2    2   40.4063  2.231175   -0.0028 -0.000146
   41.4598 2.176864   2  6  1    2   41.4596  2.176876   -0.0002 -0.000012
   43.9933 2.057159   2  0  2    2   43.9925  2.057195   -0.0008 -0.000036
   44.6101 2.030128   3  5  1    2   44.6114  2.030070    0.0013  0.000058
   55.2775 1.660850   4  6  1    2   55.2791  1.660805    0.0016  0.000045
   56.4449 1.629229   1 11  0    2   56.4409  1.629335   -0.0040 -0.000105
   64.1759 1.450304  -6  6  1    2   64.1770  1.450282    0.0011  0.000022

 rmse = 0.00004189495
 
     A =9.9238(5)              B =18.1873(9)              C =5.3301(6)           
 Alpha =90                  Beta =104.980(6)          Gamma =90                  
 
 Volume = 929.32(9)