******************************************************************************
       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 R060226_micropowder_corrected
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  0.710710
 Wavelength #2 =  0.709270
 Wavelength #3 =  0.713590
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.051
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    6.0611 6.764913   1  0  0    2    6.0530  6.774072   -0.0081 -0.009159
    9.0897 4.500758  -1  0  2    2    9.0981  4.496574    0.0084  0.004184
   12.0709 3.387157   2  0  0    2   12.0713  3.387036    0.0004  0.000121
   12.8771 3.175058  -1  1  2    2   12.8802  3.174293    0.0031  0.000766
   14.1831 2.882926  -2  1  2    2   14.1757  2.884419   -0.0074 -0.001493
   15.1293 2.702962   2  1  0    2   15.1338  2.702159    0.0045  0.000803
   22.4667 1.824559   1  1  3    2   22.4681  1.824444    0.0014  0.000115
   23.0697 1.777382  -1  2  3    2   23.0682  1.777498   -0.0015 -0.000115
   23.5845 1.739032   3  1  1    2   23.5815  1.739251   -0.0030 -0.000219
   28.4046 1.448001  -4  2  1    2   28.4062  1.447923    0.0016  0.000078

 rmse = 0.00009047385
 
     A =8.179(4)               B =4.482(2)                C =8.994(5)            
 Alpha =90                  Beta =124.09(3)           Gamma =90                  
 
 Volume = 273.0(1)