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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R040021
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.034
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    7.480211.861944   1  1  0    2    7.4772 11.866784   -0.0030 -0.004841
    9.9270 8.933069   0  2  0    2    9.9344  8.926405    0.0074  0.006665
   11.1676 7.940327   2  0  0    2   11.1655  7.941800   -0.0021 -0.001473
   13.3295 6.653689   0  0  1    2   13.3353  6.650804    0.0058  0.002885
   14.9512 5.933806   2  2  0    2   14.9522  5.933392    0.0010  0.000414
   16.6460 5.332054   0  2  1    2   16.6423  5.333235   -0.0037 -0.001181
   16.8688 5.261987  -3  1  1    2   16.8666  5.262665   -0.0022 -0.000678
   17.3330 5.121821   1  1  1    2   17.3390  5.120072    0.0060  0.001749
   17.4923 5.075444   3  1  0    2   17.4903  5.076016   -0.0020 -0.000571
   19.1338 4.642792  -1  3  1    2   19.1296  4.643802   -0.0042 -0.001010
   20.3184 4.374253  -4  0  1    2   20.3214  4.373614    0.0030  0.000639
   22.8751 3.890084   2  4  0    2   22.8704  3.890868   -0.0047 -0.000784
   23.1812 3.839330   2  2  1    2   23.1892  3.838020    0.0080  0.001309
   24.9810 3.566272  -3  1  2    2   24.9795  3.566485   -0.0015 -0.000213
   25.6252 3.477942  -5  1  1    2   25.6221  3.478356   -0.0031 -0.000414
   26.0032 3.428170  -2  2  2    2   26.0027  3.428240   -0.0005 -0.000070
   26.8295 3.324301   0  0  2    2   26.8205  3.325402   -0.0090 -0.001101
   28.0680 3.180190  -4  2  2    2   28.0716  3.179789    0.0036  0.000401
   29.0424 3.075546  -1  3  2    2   29.0476  3.075005    0.0052  0.000541

 rmse = 0.00002766241
 
     A =    17.742(2)          B =    17.852(4)           C =     7.4293(7)      
 Alpha =    90.             Beta =   116.46(1)        Gamma =    90.             
 
 Volume =   2106.7(4)