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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070539
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.092
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   25.2550 3.510997  -2  0  2    2   25.2693  3.509045    0.0143  0.001952
   40.8579 2.202099   4  0  2    2   40.8635  2.201811    0.0056  0.000288
   41.8996 2.149848   0  1  3    2   41.9043  2.149620    0.0047  0.000227
   76.9888 1.236281   4  2  0    2   76.9895  1.236271    0.0007  0.000010
   56.1179 1.635123   0  0  6    2   56.1181  1.635119    0.0002  0.000004
   25.5931 3.465542   2  0  2    2   25.5901  3.465941   -0.0030 -0.000399
   17.9833 4.903770   0  0  2    2   17.9774  4.905356   -0.0059 -0.001586
   38.8610 2.310268   3  0  3    2   38.8547  2.310627   -0.0063 -0.000359
   45.6454 1.982109  -3  1  2    2   45.6370  1.982453   -0.0084 -0.000344

 rmse = 0.00007149717
 
     A =9.918(2)               B =2.8525(3)               C =9.8115(9)           
 Alpha =90                  Beta =90.71(2)            Gamma =90                  
 
 Volume = 277.55(5)