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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R061009
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.015
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    9.6271 9.194037   0  1  0    2    9.6311  9.190237    0.0040  0.003800
   11.1638 7.929951  -1  1  0    2   11.1686  7.926541    0.0048  0.003410
   18.4546 4.807653  -1  2  0    2   18.4510  4.808574   -0.0036 -0.000921
   19.3147 4.595291   0  2  0    2   19.3154  4.595119    0.0007  0.000172
   22.4269 3.963703   0 -2  1    2   22.4269  3.963703    0.0000  0.000000
   24.5265 3.628724   1  2  0    2   24.5353  3.627436    0.0088  0.001289
   24.8973 3.575481  -2  0  1    2   24.8973  3.575481    0.0000  0.000000
   27.3763 3.256899  -1  3  0    2   27.3742  3.257138   -0.0021 -0.000240
   29.1413 3.063424   0  3  0    2   29.1414  3.063412    0.0001  0.000012
   32.1573 2.782522   2  2  0    2   32.1579  2.782473    0.0006  0.000049
   34.1346 2.625655  -1  1  3    2   34.1346  2.625655    0.0000  0.000000
   37.9523 2.369743  -4  2  0    2   37.9527  2.369721    0.0004  0.000022
   40.8133 2.209922   2  3  0    2   40.8109  2.210048   -0.0024 -0.000126
   43.8184 2.065025   1  4  0    2   43.8132  2.065257   -0.0052 -0.000232
   54.1653 1.692343   1  5  0    2   54.1685  1.692251    0.0032  0.000092

 rmse = 0.00003070067
 
     A =10.206(4)              B =9.7782(9)               C =9.658(6)            
 Alpha =92.13(4)            Beta =70.17(6)            Gamma =109.39(1)           
 
 Volume = 852.2(5)