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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050556
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.026
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   15.3946 5.760649   0  1  0    2   15.3975  5.759581    0.0029  0.001068
   18.3766 4.830703   1  0  0    2   18.3856  4.828346    0.0090  0.002357
   23.5783 3.774255   0  1  1    2   23.5783  3.774259    0.0000 -0.000004
   24.0584 3.699932   1  1  0    2   24.0569  3.700156   -0.0015 -0.000224
   29.8275 2.995511   1  1  1    2   29.8274  2.995519   -0.0001 -0.000007
   30.2789 2.951836  -1  1  1    2   30.2760  2.952110   -0.0029 -0.000274
   31.0536 2.879877   0  2  0    2   31.0546  2.879791    0.0010  0.000086
   37.2412 2.414033   2  0  0    2   37.2390  2.414173   -0.0022 -0.000140
   44.8490 2.020380  -2  1  1    2   44.8585  2.019975    0.0095  0.000404
   47.3354 1.919831   0  3  0    2   47.3346  1.919860   -0.0008 -0.000030
   48.2075 1.887098   0  2  2    2   48.2067  1.887130   -0.0008 -0.000031
   49.2425 1.849808   2  2  0    2   49.2348  1.850078   -0.0077 -0.000270
   51.1865 1.783989   1  3  0    2   51.1860  1.784004   -0.0005 -0.000015
   61.3645 1.510115  -1  1  3    2   61.3625  1.510160   -0.0020 -0.000045
   63.8585 1.456992   1  3  2    2   63.8622  1.456917    0.0037  0.000076
   67.6855 1.383589   0  4  1    2   67.6854  1.383591   -0.0001 -0.000002

 rmse = 0.00004379667
 
     A =     4.8293(4)         B =     5.7595(2)          C =     4.9975(3)      
 Alpha =    90.             Beta =    88.859(9)       Gamma =    90.             
 
 Volume =    138.97(1)