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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060718
 
 Symmetry constraint is: HEXAGONAL   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.039
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   10.0653 8.815241   1  0  1    2   10.0699  8.811219    0.0046  0.004022
   10.8938 8.144174   0  0  3    2   10.9112  8.131181    0.0174  0.012993
   11.8690 7.474888   0  1  2    2   11.8771  7.469763    0.0081  0.005125
   16.2720 5.455921   1  1  0    2   16.2733  5.455493    0.0013  0.000429
   17.3340 5.123210   1  0  4    2   17.3316  5.123926   -0.0024 -0.000716
   19.1597 4.637938   0  2  1    2   19.1578  4.638396   -0.0019 -0.000458
   19.6162 4.530806   2 -1  3    2   19.6184  4.530300    0.0022  0.000506
   20.1796 4.405315   2  0  2    2   20.1782  4.405610   -0.0014 -0.000294
   20.5012 4.336797   0  1  5    2   20.5098  4.335002    0.0086  0.001795
   21.8694 4.067980   0  0  6    2   21.8824  4.065590    0.0130  0.002390
   23.8372 3.735871   0  2  4    2   23.8436  3.734881    0.0064  0.000990
   26.0208 3.426630   1  2  2    2   26.0138  3.427535   -0.0070 -0.000906
   26.2690 3.394765   2  0  5    2   26.2753  3.393969    0.0063  0.000796
   28.9847 3.082141   3 -1  4    2   28.9875  3.081852    0.0028  0.000289
   30.4526 2.936641   0  3  3    2   30.4480  2.937073   -0.0046 -0.000432
   30.8252 2.901942   0  1  8    2   30.8262  2.901847    0.0010  0.000095
   31.0450 2.881870  -1  3  5    2   31.0457  2.881804    0.0007  0.000065
   31.9149 2.805178   0  2  7    2   31.9233  2.804456    0.0084  0.000722
   32.8499 2.727343   2  2  0    2   32.8449  2.727746   -0.0050 -0.000403
   34.4231 2.606070   1  3  1    2   34.4276  2.605739    0.0045  0.000331
   34.7044 2.585563   4 -2  3    2   34.6969  2.586107   -0.0075 -0.000543
   37.3646 2.407171   1  3  4    2   37.3543  2.407813   -0.0103 -0.000642
   40.9779 2.202664   4  0  4    2   40.9752  2.202805   -0.0027 -0.000141
   45.0037 2.014358   3 -1 10    2   45.0041  2.014340    0.0004  0.000018
   56.4439 1.629931   2  2 12    2   56.4427  1.629961   -0.0012 -0.000031
   73.1355 1.293511   2  4 13    2   73.1312  1.293577   -0.0043 -0.000066
   79.5906 1.203974   2  6  8    2   79.5959  1.203906    0.0053  0.000067

 rmse = 0.00004359497
 
     A =    10.9109(4)         B =    10.9109(4)          C =    24.393(1)       
 Alpha =    90.             Beta =    90.             Gamma =   120.             
 
 Volume =   2514.9(1)