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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050520
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.046
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   14.7139 6.034127   1  1  0    2   14.7200  6.031617    0.0061  0.002510
   18.5491 4.791168   0  0  1    2   18.5492  4.791151    0.0001  0.000017
   21.5935 4.120626   2  1  0    2   21.5999  4.119412    0.0064  0.001214
   21.9031 4.062953   0  1  1    2   21.9016  4.063228   -0.0015 -0.000275
   23.2199 3.834981   0  2  0    2   23.2255  3.834064    0.0056  0.000917
   29.8717 2.993112   0  2  1    2   29.8672  2.993552   -0.0045 -0.000441
   36.8226 2.441794   4  0  0    2   36.8192  2.442010   -0.0034 -0.000216
   38.7114 2.326749   4  1  0    2   38.7094  2.326866   -0.0020 -0.000117
   43.1964 2.094727  -4  1  1    2   43.1987  2.094620    0.0023  0.000108
   44.2349 2.047878  -2  3  1    2   44.2282  2.048172   -0.0067 -0.000294
   45.1023 2.010448   3  3  0    2   45.1002  2.010539   -0.0021 -0.000091
   47.4207 1.917327   0  4  0    2   47.4285  1.917032    0.0078  0.000296
   52.5732 1.740736   5  2  0    2   52.5754  1.740667    0.0022  0.000068
   74.1777 1.277979   0  6  0    2   74.1748  1.278021   -0.0029 -0.000043
   76.7858 1.240913   6  4  0    2   76.7859  1.240912    0.0001  0.000001
   86.9228 1.120286  -1  6  2    2   86.9243  1.120270    0.0015  0.000015

 rmse = 0.00004155154
 
     A =     9.7680(4)         B =     7.6681(2)          C =     4.7911(8)      
 Alpha =    90.             Beta =    90.11(2)        Gamma =    90.             
 
 Volume =    358.87(6)