Julgoldite-(Fe3+) Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from the powder pattern Artioli G, Geiger C A, Dapiaggi M American Mineralogist 88 (2003) 1084-1090 The crystal chemistry of julgoldite-Fe3+ from Bombay, India, studied using synchrotron X-ray powder diffraction and 57Fe Mossbauer spectroscopy CELL PARAMETERS: 8.911716 6.066097 19.37995 90.00000 97.58549 90.00000 SPACE GROUP: A2/m X-RAY WAVELENGTH: 1.541838 2-THETA INTENSITY D-SPACING H K L 9.21 32.47 9.6052 0 0 2 10.02 14.57 8.8337 1 0 0 12.69 5.68 6.9771 -1 0 2 14.49 9.89 6.1124 1 0 2 17.99 5.72 4.9300 -1 1 1 18.47 51.26 4.8026 0 0 4 18.67 32.20 4.7535 1 1 1 19.84 12.95 4.4745 -1 0 4 20.10 22.43 4.4169 2 0 0 21.00 3.84 4.2305 -2 0 2 21.71 7.54 4.0924 -1 1 3 22.20 4.57 4.0034 1 0 4 23.25 86.85 3.8258 2 0 2 23.37 4.93 3.8057 1 1 3 24.87 2.39 3.5798 -2 1 1 25.53 25.86 3.4886 -2 0 4 25.85 4.66 3.4451 2 1 1 27.26 1.77 3.2706 -2 1 3 28.20 3.75 3.1630 -1 1 5 29.21 21.27 3.0562 2 0 4 29.44 2.60 3.0330 0 2 0 29.91 5.54 2.9860 2 1 3 30.37 83.35 2.9423 1 1 5 30.34 16.65 2.9446 3 0 0 30.55 20.11 2.9256 -3 0 2 30.91 22.92 2.8923 0 2 2 30.93 2.55 2.8904 1 0 6 31.17 16.35 2.8687 1 2 0 32.17 11.22 2.7816 -1 2 2 32.28 80.43 2.7720 -2 0 6 32.34 2.86 2.7669 -2 1 5 32.95 14.21 2.7169 1 2 2 32.96 2.34 2.7166 3 0 2 33.52 1.15 2.6724 -3 0 4 33.58 34.82 2.6674 -3 1 1 34.72 1.56 2.5830 3 1 1 34.97 85.84 2.5644 0 2 4 35.75 7.59 2.5106 -1 2 4 35.90 27.77 2.5003 2 2 0 36.11 2.74 2.4865 2 1 5 36.12 26.27 2.4855 -1 1 7 36.43 24.28 2.4650 -2 2 2 36.76 3.96 2.4435 2 0 6 37.17 1.84 2.4176 1 2 4 37.43 7.67 2.4013 0 0 8 37.48 4.92 2.3987 -1 0 8 37.84 59.06 2.3768 2 2 2 38.26 15.37 2.3512 3 1 3 38.57 1.69 2.3334 1 1 7 38.70 2.53 2.3257 -3 0 6 38.92 7.49 2.3130 -3 1 5 40.29 32.41 2.2372 -2 0 8 40.67 3.47 2.2171 -4 0 2 40.84 12.30 2.2084 4 0 0 40.97 4.47 2.2019 0 2 6 41.33 4.96 2.1836 -1 2 6 41.95 31.66 2.1528 2 2 4 42.73 18.65 2.1152 -4 0 4 42.78 2.13 2.1127 3 2 0 42.93 1.10 2.1057 -3 2 2 43.22 3.68 2.0924 1 2 6 43.24 3.58 2.0911 -4 1 1 44.61 3.26 2.0302 -3 1 7 46.42 3.47 1.9549 1 3 1 46.76 6.45 1.9417 -4 0 6 47.09 1.09 1.9286 -4 1 5 47.51 1.57 1.9129 4 0 4 47.52 3.22 1.9122 1 1 9 47.69 4.80 1.9060 4 1 3 47.77 19.46 1.9028 2 2 6 48.32 30.09 1.8827 0 2 8 48.35 6.15 1.8815 -1 2 8 48.67 5.53 1.8697 3 2 4 49.13 1.31 1.8534 -2 0 10 49.35 3.09 1.8456 -3 2 6 50.67 1.18 1.8004 -2 2 8 50.99 3.32 1.7899 -4 2 2 51.13 6.46 1.7853 4 2 0 51.71 1.36 1.7667 5 0 0 51.80 4.19 1.7638 -4 1 7 52.21 3.30 1.7512 3 0 8 52.43 2.36 1.7443 -4 0 8 52.63 6.21 1.7380 4 1 5 52.73 22.27 1.7350 -4 2 4 52.79 7.73 1.7331 1 3 5 53.14 1.77 1.7225 4 2 2 53.39 6.44 1.7152 4 0 6 53.36 3.58 1.7159 -3 0 10 53.96 1.23 1.6982 5 0 2 54.12 4.94 1.6937 -5 1 3 54.30 6.04 1.6885 -1 1 11 54.90 9.82 1.6714 -3 3 1 56.22 1.41 1.6353 -4 2 6 56.65 2.63 1.6237 -1 3 7 56.69 6.93 1.6229 0 2 10 56.87 52.31 1.6180 4 2 4 57.06 1.89 1.6130 -1 0 12 57.54 19.43 1.6009 0 0 12 57.98 2.47 1.5897 -4 1 9 58.19 1.76 1.5845 3 3 3 58.31 28.03 1.5815 -2 2 10 58.67 2.44 1.5727 -3 3 5 58.65 1.42 1.5730 -2 0 12 58.97 4.84 1.5655 1 2 10 59.42 1.37 1.5546 -4 0 10 60.25 2.38 1.5351 -5 2 2 60.37 1.09 1.5324 -5 1 7 60.55 12.78 1.5281 4 0 8 60.62 1.58 1.5266 5 2 0 60.81 1.45 1.5222 -5 0 8 60.92 1.84 1.5197 3 0 10 61.07 35.56 1.5165 0 4 0 61.27 27.77 1.5121 -4 2 8 61.57 5.92 1.5053 -5 2 4 62.51 1.68 1.4849 -6 0 2 63.16 13.98 1.4711 2 2 10 64.38 2.33 1.4461 0 4 4 64.43 1.36 1.4452 2 0 12 65.34 5.76 1.4273 6 0 2 65.47 1.67 1.4247 4 3 3 65.50 3.16 1.4241 -1 2 12 65.94 3.09 1.4158 0 2 12 66.25 6.04 1.4098 2 4 2 66.23 3.32 1.4102 -6 0 6 67.28 2.17 1.3908 -2 4 4 67.54 7.99 1.3860 -4 0 12 68.74 1.98 1.3647 4 2 8 68.88 1.75 1.3623 -4 3 7 68.95 1.98 1.3611 -3 1 13 68.98 1.71 1.3605 -5 2 8 69.10 2.01 1.3585 2 4 4 69.58 2.50 1.3503 4 3 5 69.70 2.22 1.3482 3 4 0 69.81 2.77 1.3464 -3 4 2 70.53 1.95 1.3345 3 0 12 70.57 9.81 1.3337 -6 2 2 70.77 11.88 1.3304 -2 4 6 70.85 3.29 1.3292 -5 3 3 71.00 2.46 1.3267 -1 3 11 71.14 1.50 1.3245 6 2 0 71.57 7.00 1.3176 -6 2 4 71.93 1.11 1.3118 -3 0 14 72.56 1.21 1.3020 -5 1 11 73.44 1.71 1.2885 2 4 6 73.86 2.12 1.2822 0 4 8 74.10 1.87 1.2787 -6 2 6 74.20 1.42 1.2771 -4 3 9 74.33 2.45 1.2753 6 0 6 74.48 1.22 1.2731 -7 0 2 74.85 1.23 1.2677 -5 2 10 75.11 7.15 1.2640 2 0 14 75.14 2.27 1.2635 -1 1 15 75.72 4.82 1.2553 -2 4 8 75.89 1.83 1.2529 5 1 9 76.09 3.26 1.2501 4 4 0 76.08 3.60 1.2502 0 2 14 76.02 1.05 1.2510 -6 0 10 76.62 1.45 1.2427 -2 2 14 77.38 3.89 1.2325 -4 4 4 77.82 2.03 1.2265 5 2 8 78.18 1.29 1.2218 4 0 12 78.50 1.28 1.2177 1 2 14 80.27 1.32 1.1952 -4 4 6 81.89 1.39 1.1756 6 2 6 82.05 1.83 1.1737 -5 2 12 82.66 1.05 1.1666 2 1 15 84.19 1.31 1.1492 -3 3 13 84.45 1.22 1.1464 3 4 8 84.91 3.77 1.1413 1 5 5 85.01 1.72 1.1402 7 2 2 85.39 2.05 1.1361 4 4 6 85.37 1.39 1.1363 -3 4 10 85.60 1.43 1.1339 5 2 10 85.65 1.41 1.1333 4 2 12 86.45 1.60 1.1249 -1 2 16 86.62 1.03 1.1231 -3 5 1 87.27 3.97 1.1164 0 2 16 87.53 1.34 1.1138 -8 0 2 88.07 2.11 1.1083 -1 5 7 88.04 2.07 1.1086 -8 0 4 88.34 2.57 1.1056 6 2 8 88.48 1.63 1.1042 8 0 0 88.71 1.38 1.1019 7 2 4 88.81 7.79 1.1010 0 4 12 88.86 1.44 1.1005 6 0 10 89.36 1.33 1.0956 3 5 3 89.36 1.33 1.0956 3 5 3 XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.