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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 R060933.1__Powder__Xray_Data_XY_Processed__7161[1]
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.095
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   40.8512 2.212085   5  1  2    2   40.8358  2.212887   -0.0154 -0.000802
   41.3998 2.183963   1  4  2    2   41.3964  2.184137   -0.0034 -0.000174
   17.0939 5.211605   0  2  0    2   17.0981  5.210329    0.0042  0.001276
   48.7496 1.869842   2  2  4    2   48.7444  1.870032   -0.0052 -0.000189
   63.3023 1.469886   6  2  4    2   63.3084  1.469760    0.0061  0.000127
   30.4683 2.940391   3  1  2    2   30.4775  2.939520    0.0092  0.000872
   22.2564 4.007860   1  0  2    2   22.2610  4.007042    0.0046  0.000818
   21.6330 4.122434   2  2  0    2   21.6540  4.118463    0.0210  0.003971

 rmse = 0.00010130382
 
     A =13.447(4)              B =10.421(4)               C =8.395(2)            
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 1176.5(4)