Kasolite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from single crystal data for R060479 Mokeeva V I Soviet Physics - Crystallography 9 (1965) 621-622 The crystal structure of kasolite CELL PARAMETERS: 13.2800 6.9600 6.7400 90.000 75.750 90.000 SPACE GROUP: P2_1/a ATOM X Y Z OCCUPANCY ISO(B) Pb 0.11700 0.57000 0.07300 1.000 2.000 U 0.18000 0.24600 0.52600 1.000 2.000 Si 0.08000 0.75000 0.58000 1.000 2.000 O 0.03000 0.75000 0.83000 1.000 2.000 O -0.01000 0.75000 0.45000 1.000 2.000 O 0.16000 0.94000 0.51000 1.000 2.000 O 0.16000 0.56000 0.51000 1.000 2.000 O 0.18000 0.25000 0.27000 1.000 2.000 O 0.18000 0.25000 0.78000 1.000 2.000 X-RAY WAVELENGTH: 1.541838 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 11 +/- 6 +/- 5 MAX. ABS. INTENSITY / VOLUME**2: 75.77276643 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 13.55 32.60 6.5326 0 0 1 13.76 28.40 6.4357 2 0 0 14.47 75.29 6.1223 1 1 0 16.79 18.71 5.2802 2 0 1 18.63 5.42 4.7632 0 1 1 18.67 11.23 4.7534 1 1 1 18.78 12.23 4.7252 2 1 0 21.02 57.23 4.2270 -1 1 1 21.12 57.26 4.2066 2 1 1 21.64 30.08 4.1070 -2 0 1 24.37 13.09 3.6523 3 1 0 25.18 72.74 3.5371 -2 1 1 25.32 31.42 3.5172 3 1 1 25.60 15.74 3.4800 0 2 0 26.53 13.02 3.3594 1 2 0 27.30 58.59 3.2663 0 0 2 27.41 49.53 3.2538 2 0 2 27.72 27.95 3.2178 4 0 0 27.72 9.09 3.2176 4 0 1 29.07 91.65 3.0714 0 2 1 29.10 13.91 3.0688 1 2 1 29.17 10.69 3.0611 2 2 0 30.61 58.65 2.9208 4 1 0 30.61 41.35 2.9206 4 1 1 30.77 25.79 2.9057 2 2 1 32.55 17.59 2.7512 -1 1 2 32.73 17.75 2.7362 3 1 2 33.15 8.11 2.7027 3 2 0 33.69 3.93 2.6603 -2 0 2 33.87 2.94 2.6466 3 2 1 33.95 1.72 2.6405 -4 0 1 33.96 6.28 2.6401 4 0 2 36.15 4.63 2.4850 -2 1 2 36.39 10.69 2.4688 -4 1 1 36.40 3.96 2.4685 4 1 2 36.58 3.64 2.4566 5 1 1 37.14 10.71 2.4209 1 2 2 37.24 10.06 2.4144 5 1 0 37.77 3.64 2.3816 0 2 2 37.85 1.33 2.3767 2 2 2 37.95 8.63 2.3709 -3 2 1 38.09 4.21 2.3626 4 2 0 38.09 7.10 2.3625 4 2 1 40.92 3.03 2.2054 6 0 1 41.30 1.40 2.1862 0 3 1 41.37 42.06 2.1825 2 3 0 41.47 6.55 2.1775 0 0 3 42.12 4.57 2.1452 6 0 0 42.40 2.29 2.1320 1 1 3 42.45 2.30 2.1293 2 1 3 42.79 5.09 2.1135 -2 2 2 42.82 7.92 2.1117 -5 1 1 43.00 5.01 2.1035 -4 2 1 43.00 3.62 2.1033 4 2 2 43.02 1.41 2.1024 6 1 1 43.16 3.81 2.0960 5 2 1 43.55 7.22 2.0782 0 1 3 43.71 6.70 2.0709 3 1 3 43.74 1.71 2.0696 5 2 0 44.10 4.18 2.0535 -4 0 2 44.11 1.70 2.0532 4 0 3 44.18 8.64 2.0501 6 1 0 44.45 8.40 2.0380 6 0 2 45.83 4.55 1.9798 -1 1 3 46.09 14.44 1.9695 -4 1 2 46.09 14.53 1.9693 4 1 3 46.43 13.07 1.9559 6 1 2 46.83 4.20 1.9398 -3 2 2 47.10 4.54 1.9293 5 2 2 47.24 3.86 1.9239 -2 0 3 47.77 12.44 1.9040 -6 0 1 48.11 8.16 1.8914 0 3 2 48.17 11.19 1.8890 2 3 2 48.33 2.50 1.8833 1 2 3 48.37 11.24 1.8819 4 3 0 48.37 7.11 1.8818 4 3 1 48.38 17.27 1.8815 2 2 3 48.89 3.46 1.8628 6 2 1 49.13 7.44 1.8544 -2 1 3 49.37 8.14 1.8459 0 2 3 49.85 2.99 1.8292 7 1 1 49.94 8.02 1.8261 6 2 0 51.46 1.34 1.7759 -1 2 3 52.04 3.86 1.7573 -5 1 2 52.32 11.07 1.7485 -2 3 2 52.42 4.11 1.7456 7 1 2 52.51 16.42 1.7428 -4 3 1 52.51 13.10 1.7427 4 3 2 52.60 4.51 1.7400 0 4 0 53.11 1.53 1.7243 1 4 0 53.30 1.66 1.7186 -3 1 3 53.72 3.64 1.7064 6 1 3 54.46 13.51 1.6849 2 0 4 54.50 1.94 1.6837 -2 2 3 54.58 8.88 1.6814 0 4 1 54.60 4.64 1.6809 1 4 1 54.64 1.67 1.6797 2 4 0 54.82 2.27 1.6747 5 2 3 54.97 1.13 1.6703 -6 2 1 55.17 1.24 1.6649 7 2 1 55.34 9.84 1.6600 8 0 1 55.61 3.25 1.6526 2 4 1 56.33 1.24 1.6332 0 0 4 56.60 2.23 1.6261 1 1 4 56.61 1.62 1.6258 7 2 0 56.72 1.16 1.6230 3 1 4 57.12 2.54 1.6124 3 4 0 57.67 10.71 1.5984 6 3 1 58.23 1.15 1.5844 -4 1 3 58.40 1.08 1.5802 -3 2 3 58.71 2.56 1.5726 7 1 3 58.79 4.14 1.5706 6 2 3 58.92 1.41 1.5676 8 1 0 59.82 2.41 1.5461 1 4 2 60.27 2.58 1.5357 0 4 2 60.32 1.63 1.5344 2 4 2 60.39 2.83 1.5328 -3 4 1 60.68 1.16 1.5261 5 1 4 61.11 1.37 1.5165 2 2 4 61.63 1.20 1.5049 3 2 4 61.72 1.94 1.5029 -7 2 1 61.97 1.28 1.4975 -2 0 4 62.41 3.49 1.4879 6 0 4 62.74 3.29 1.4809 -2 3 3 62.79 3.54 1.4799 -8 0 1 62.80 3.47 1.4798 8 0 3 62.86 2.64 1.4784 0 2 4 63.17 2.67 1.4718 -6 3 1 63.34 5.30 1.4683 -6 2 2 63.55 5.42 1.4640 -2 1 4 63.73 7.68 1.4604 8 2 0 63.73 4.95 1.4603 8 2 2 63.99 4.40 1.4550 6 1 4 64.22 1.87 1.4504 5 4 1 65.09 1.02 1.4330 -1 2 4 66.70 4.98 1.4022 6 3 3 66.78 1.62 1.4009 9 1 0 67.07 1.82 1.3955 -3 4 2 67.28 1.83 1.3916 5 4 2 67.56 1.53 1.3865 -3 1 4 68.26 1.77 1.3740 1 4 3 68.30 3.01 1.3733 2 4 3 68.55 5.10 1.3690 -6 0 3 68.71 1.13 1.3660 6 4 1 69.10 2.39 1.3593 0 4 3 69.57 2.13 1.3514 6 4 0 69.88 2.75 1.3460 2 5 1 70.52 4.35 1.3355 0 3 4 70.72 7.18 1.3321 -4 3 3 70.73 6.97 1.3320 4 3 4 71.34 1.15 1.3220 8 3 2 71.57 3.78 1.3183 -2 5 1 72.14 1.31 1.3094 1 1 5 72.31 1.20 1.3067 -9 1 1 72.32 1.50 1.3065 0 0 5 72.32 2.15 1.3065 -4 1 4 72.33 1.51 1.3064 4 1 5 72.93 1.60 1.2971 -8 1 2 73.39 1.69 1.2901 10 1 2 73.64 1.30 1.2864 5 4 3 73.77 1.20 1.2844 -6 4 1 73.79 1.87 1.2841 0 1 5 74.11 1.13 1.2793 5 1 5 74.23 2.88 1.2776 4 5 0 74.23 2.37 1.2776 4 5 1 75.05 2.73 1.2657 10 1 0 75.18 1.37 1.2638 7 4 0 75.57 1.59 1.2582 -2 3 4 75.73 3.84 1.2559 2 2 5 75.98 2.09 1.2525 6 3 4 76.08 1.71 1.2511 10 0 3 76.32 2.87 1.2477 -8 3 1 76.70 1.16 1.2425 -4 2 4 76.71 1.17 1.2424 4 2 5 76.72 2.57 1.2422 6 1 5 77.30 1.35 1.2344 -8 2 2 77.31 1.68 1.2342 8 2 4 77.75 1.50 1.2283 10 2 2 79.12 1.54 1.2104 2 4 4 81.13 1.30 1.1855 -6 4 2 81.48 1.84 1.1813 8 4 0 81.48 1.17 1.1813 8 4 2 82.19 1.47 1.1728 0 5 3 82.63 1.75 1.1677 6 5 0 83.30 2.71 1.1600 0 6 0 83.99 2.60 1.1522 -4 5 2 84.00 2.57 1.1522 4 5 3 84.06 3.15 1.1514 10 3 1 84.24 2.36 1.1495 6 5 2 86.25 1.00 1.1278 -2 5 3 87.15 1.24 1.1184 -4 0 5 88.23 2.61 1.1075 -6 2 4 88.86 1.75 1.1012 10 3 3 89.02 2.26 1.0997 10 2 4 89.70 2.01 1.0931 0 6 2 89.75 1.83 1.0926 2 6 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.