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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050214
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.034
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   11.0756 8.006802   2  0  0    2   11.0815  8.002566    0.0059  0.004237
   12.9260 6.861398   0  2  0    2   12.9343  6.857007    0.0083  0.004392
   17.0447 5.208191   2  2  0    2   17.0487  5.206978    0.0040  0.001212
   21.6178 4.113898   2  2  1    2   21.6202  4.113447    0.0024  0.000451
   22.2383 4.000315   4  0  0    2   22.2329  4.001283   -0.0054 -0.000967
   24.2183 3.677094   1  3  1    2   24.2208  3.676716    0.0025  0.000378
   25.9946 3.429380   0  4  0    2   26.0014  3.428503    0.0068  0.000877
   26.5856 3.354371   0  0  2    2   26.5845  3.354503   -0.0011 -0.000131
   29.2617 3.053041   0  4  1    2   29.2625  3.052959    0.0008  0.000082
   29.6585 3.013044   0  2  2    2   29.6564  3.013253   -0.0021 -0.000209
   32.1968 2.780807   3  1  2    2   32.1969  2.780800    0.0001  0.000007
   33.1423 2.703521   1  5  0    2   33.1439  2.703394    0.0016  0.000127
   34.2060 2.621759   5  3  0    2   34.2016  2.622089   -0.0044 -0.000330
   37.5064 2.398077   0  4  2    2   37.5121  2.397727    0.0057  0.000350
   42.5201 2.125960   0  2  3    2   42.5168  2.126118   -0.0033 -0.000158
   42.9640 2.105000   6  4  0    2   42.9566  2.105344   -0.0074 -0.000344
   45.6020 1.989081   5  5  1    2   45.6005  1.989142   -0.0015 -0.000060
   48.5962 1.873205   0  4  3    2   48.5994  1.873089    0.0032  0.000115
   51.6454 1.769470   5  5  2    2   51.6457  1.769461    0.0003  0.000009
   54.7189 1.677060   0  0  4    2   54.7121  1.677251   -0.0068 -0.000192
   57.5694 1.600563  10  0  0    2   57.5714  1.600513    0.0020  0.000050
   59.9900 1.541598   6  6  2    2   59.9926  1.541536    0.0026  0.000061
   62.0274 1.495734   5  7  2    2   62.0284  1.495711    0.0010  0.000022
   66.1066 1.412926   5  3  4    2   66.1071  1.412918    0.0005  0.000009
   69.4793 1.352316   0  6  4    2   69.4840  1.352235    0.0047  0.000081
   74.7550 1.269363   0 10  2    2   74.7514  1.269415   -0.0036 -0.000052

 rmse = 0.00003750315
 
     A =    16.0051(6)         B =    13.7140(4)          C =     6.7090(2)      
 Alpha =    90.             Beta =    90.             Gamma =    90.             
 
 Volume =   1472.59(6)