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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070284
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.029
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    9.2502 9.582753   2  0  0    2    9.2594  9.573237    0.0092  0.009516
   18.7439 4.737510   3  1  0    2   18.7345  4.739873   -0.0094 -0.002363
   23.9857 3.711468  -3  1  1    2   23.9934  3.710287    0.0077  0.001181
   26.2070 3.401354   3  1  1    2   26.2066  3.401402   -0.0004 -0.000048
   26.4666 3.368541   5  1  0    2   26.4709  3.368002    0.0043  0.000539
   27.9693 3.190691   6  0  0    2   27.9658  3.191079   -0.0035 -0.000388
   29.8554 2.993078  -5  1  1    2   29.8642  2.992217    0.0088  0.000860
   30.9177 2.892520  -6  0  1    2   30.9065  2.893542   -0.0112 -0.001022
   31.4365 2.845913   4  2  0    2   31.4388  2.845708    0.0023  0.000204
   32.3204 2.770002   2  2  1    2   32.3265  2.769495    0.0061  0.000506
   32.8782 2.724228   5  1  1    2   32.8697  2.724916   -0.0085 -0.000688
   34.3860 2.608043   6  0  1    2   34.3865  2.608006    0.0005  0.000037
   35.1703 2.551611   7  1  0    2   35.1741  2.551341    0.0038  0.000270
   36.5367 2.459183  -4  0  2    2   36.5376  2.459126    0.0009  0.000058
   37.5742 2.393577   8  0  0    2   37.5786  2.393309    0.0044  0.000268
   39.4032 2.286501  -8  0  1    2   39.3974  2.286826   -0.0058 -0.000326
   45.1287 2.008629   5  3  0    2   45.1269  2.008705   -0.0018 -0.000075
   51.6394 1.769493   0  4  0    2   51.6382  1.769531   -0.0012 -0.000037
   64.5421 1.443257 -12  2  1    2   64.5433  1.443233    0.0012  0.000024

 rmse = 0.00004532435
 
     A =19.2802(9)             B =7.0781(4)               C =5.3805(8)           
 Alpha =90                  Beta =96.753(8)           Gamma =90                  
 
 Volume = 729.2(1)