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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 R060130
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.061
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    9.4003 9.461655   1  0  0    2    9.4057  9.456179    0.0054  0.005476
   18.3417 4.848998   1  1  0    2   18.3443  4.848319    0.0026  0.000679
   19.6704 4.523333  -1  0  1    2   19.6683  4.523821   -0.0021 -0.000487
   24.5941 3.625531   2  1  0    2   24.5964  3.625193    0.0023  0.000338
   25.0988 3.553581   0  1  1    2   25.0976  3.553755   -0.0012 -0.000174
   28.7744 3.106497  -2  1  1    2   28.7754  3.106395    0.0010  0.000102
   30.0564 2.976581   2  0  1    2   30.0529  2.976921   -0.0035 -0.000341
   31.7161 2.824200   0  2  0    2   31.7239  2.823520    0.0078  0.000679
   33.1328 2.706384   1  2  0    2   33.1440  2.705490    0.0112  0.000895
   34.7027 2.587245  -3  1  1    2   34.7043  2.587131    0.0016  0.000114
   38.4497 2.342891  -1  0  2    2   38.4511  2.342808    0.0014  0.000083
   38.8863 2.317544  -4  0  1    2   38.8865  2.317535    0.0002  0.000009
   41.7686 2.163803  -1  1  2    2   41.7653  2.163967   -0.0033 -0.000164
   43.0370 2.102832   3  2  0    2   43.0307  2.103124   -0.0063 -0.000292
   44.2327 2.048643   2  2  1    2   44.2333  2.048615    0.0006  0.000028
   47.8754 1.900724   2  0  2    2   47.8567  1.901422   -0.0187 -0.000698
   49.3815 1.846148   1  3  0    2   49.3821  1.846126    0.0006  0.000022
   49.8547 1.829706   4  1  1    2   49.8531  1.829763   -0.0016 -0.000056
   59.5210 1.553256  -4  2  2    2   59.5235  1.553198    0.0025  0.000059
   60.0244 1.541414  -6  1  1    2   60.0278  1.541336    0.0034  0.000078
   60.7611 1.524458   0  0  3    2   60.7696  1.524264    0.0085  0.000194
   62.3804 1.488680   4  0  2    2   62.3906  1.488461    0.0102  0.000220
   65.6949 1.421295  -5  2  2    2   65.6842  1.421502   -0.0107 -0.000207
   70.9945 1.327543   2  1  3    2   70.9898  1.327619   -0.0047 -0.000076
   72.5521 1.302807  -5  1  3    2   72.5553  1.302758    0.0032  0.000049

 rmse = 0.00007551914
 
     A =9.6921(7)              B =5.6470(5)               C =4.6869(3)           
 Alpha =90                  Beta =102.667(4)          Gamma =90                  
 
 Volume = 250.28(2)