Mammothite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from single crystal data of R130100 Effenberger H Tschermaks Mineralogische und Petrographische Mitteilungen 34 (1985) 279-288 The crystal structure of mammothite, Pb6Cu4AlSbO2(OH)16Cl4(SO4)2 Locality: Mammoth vein, Tiger, Arizona, USA _database_code_amcsd 0015702 CELL PARAMETERS: 18.9610 7.3338 11.3460 90.000 112.414 90.000 SPACE GROUP: C2/m ATOM X Y Z OCCUPANCY ISO(B) Pb 0.21037 0.00000 0.17947 1.000 1.413 Pb 0.42277 0.25855 0.20296 1.000 1.492 Cu 0.25000 0.25000 0.50000 1.000 1.224 Cu 0.10420 0.00000 0.36850 1.000 1.192 Al 0.00000 0.00000 0.50000 1.000 0.711 Sb 0.00000 0.00000 0.00000 1.000 1.129 O 0.00210 0.00000 -0.16950 1.000 1.184 OH 0.23860 0.00000 -0.43930 1.000 1.500 OH 0.08720 0.00000 -0.34420 1.000 1.342 OH 0.08310 0.18540 0.04260 1.000 1.500 OH 0.04090 0.17170 0.41730 1.000 1.263 OH 0.16950 0.18330 0.33980 1.000 1.105 Cl 0.36790 0.00000 0.39630 1.000 2.369 Cl 0.44910 0.00000 -0.19950 1.000 1.816 S 0.24970 0.00000 -0.09530 1.000 1.184 O 0.17760 0.00000 -0.07090 1.000 1.579 O 0.31030 0.00000 0.02980 1.000 2.842 O 0.24820 0.15960 -0.16860 1.000 2.685 X-RAY WAVELENGTH: 1.541838 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 16 +/- 6 +/- 9 MAX. ABS. INTENSITY / VOLUME**2: 37.46898419 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 8.43 62.28 10.4888 0 0 1 10.09 3.08 8.7643 2 0 0 10.40 16.85 8.5087 -2 0 1 13.09 84.58 6.7655 1 1 0 14.50 59.27 6.1097 -1 1 1 15.45 30.96 5.7350 2 0 1 16.05 37.98 5.5228 -2 0 2 16.61 16.68 5.3388 1 1 1 16.91 43.29 5.2444 0 0 2 18.73 8.08 4.7388 -3 1 1 18.73 58.32 4.7366 -4 0 1 19.42 3.60 4.5698 3 1 0 19.83 3.29 4.4762 -1 1 2 20.26 3.55 4.3821 4 0 0 20.88 5.03 4.2543 -4 0 2 23.44 2.49 3.7955 3 1 1 23.53 24.59 3.7813 -2 0 3 24.83 57.30 3.5862 4 0 1 25.48 42.28 3.4963 0 0 3 25.74 1.61 3.4615 0 2 1 25.84 5.41 3.4481 -4 0 3 26.35 25.55 3.3828 2 2 0 26.47 15.61 3.3675 -2 2 1 26.49 2.48 3.3651 -5 1 1 27.10 42.41 3.2905 -3 1 3 28.21 13.02 3.1629 5 1 0 28.42 1.47 3.1408 -6 0 1 28.76 25.28 3.1046 -6 0 2 28.90 100.00 3.0894 2 2 1 29.23 94.63 3.0549 -2 2 2 29.51 36.69 3.0271 3 1 2 29.73 11.24 3.0052 0 2 2 30.46 1.70 2.9349 1 1 3 30.60 31.50 2.9214 6 0 0 30.84 79.23 2.8995 -4 2 1 30.92 16.07 2.8922 -5 1 3 31.19 28.53 2.8675 4 0 2 31.54 22.88 2.8362 -6 0 3 31.67 15.28 2.8254 -2 0 4 31.82 11.25 2.8122 4 2 0 32.23 2.29 2.7775 -4 2 2 32.25 8.55 2.7758 5 1 1 32.42 35.57 2.7614 -4 0 4 33.57 1.25 2.6694 2 2 2 33.97 14.52 2.6394 -3 1 4 34.83 4.90 2.5761 -1 1 4 34.88 1.67 2.5722 6 0 1 35.48 9.80 2.5304 0 2 3 35.50 11.08 2.5289 -7 1 2 35.74 21.55 2.5120 -4 2 3 36.27 6.38 2.4765 -6 0 4 37.38 5.42 2.4058 -7 1 3 37.69 7.36 2.3868 -1 3 1 37.71 25.99 2.3854 -6 2 1 37.97 3.85 2.3697 7 1 0 37.98 1.67 2.3694 -6 2 2 37.99 12.62 2.3683 -8 0 2 38.58 17.75 2.3335 4 0 3 38.60 3.65 2.3324 1 3 1 38.61 3.52 2.3321 1 1 4 39.44 24.51 2.2849 6 2 0 39.71 39.04 2.2699 2 2 3 39.91 6.55 2.2588 4 2 2 40.19 4.00 2.2436 -1 3 2 40.20 30.23 2.2435 -6 2 3 40.21 1.18 2.2429 -2 0 5 40.30 14.50 2.2381 -2 2 4 40.68 2.66 2.2178 6 0 2 41.10 1.38 2.1960 -7 1 4 41.20 1.96 2.1911 8 0 0 42.38 7.87 2.1330 0 2 4 42.39 8.11 2.1321 -6 0 5 42.50 1.53 2.1272 -8 0 4 42.75 2.38 2.1152 -5 1 5 43.12 19.61 2.0978 0 0 5 44.09 6.07 2.0539 -5 3 1 44.49 6.25 2.0366 -3 3 3 44.76 3.67 2.0248 -9 1 2 44.77 2.51 2.0245 5 1 3 45.22 5.51 2.0052 5 3 0 45.40 2.95 1.9977 8 0 1 45.60 9.65 1.9894 -8 2 2 46.09 7.58 1.9692 3 3 2 46.16 9.61 1.9665 -8 2 1 46.31 1.00 1.9606 -7 1 5 46.66 4.70 1.9467 4 0 4 46.75 1.61 1.9432 1 3 3 46.76 1.98 1.9428 -8 2 3 46.86 18.54 1.9389 2 2 4 47.07 10.28 1.9306 -5 3 3 47.19 1.83 1.9258 -8 0 5 47.21 4.33 1.9251 1 1 5 47.30 9.22 1.9219 -4 2 5 47.52 11.91 1.9134 -2 2 5 47.57 6.16 1.9117 6 0 3 47.94 10.25 1.8977 6 2 2 48.02 1.93 1.8948 5 3 1 48.05 1.30 1.8936 -10 0 2 48.31 5.41 1.8840 2 0 5 48.35 5.82 1.8824 9 1 0 48.39 5.64 1.8809 8 2 0 48.41 2.13 1.8803 -10 0 3 49.10 2.74 1.8554 -2 0 6 49.26 2.90 1.8497 -3 3 4 49.33 12.50 1.8472 -10 0 1 49.45 4.33 1.8432 -6 2 5 49.54 12.26 1.8400 -8 2 4 49.73 24.82 1.8334 0 4 0 49.90 4.71 1.8275 -1 3 4 50.20 1.89 1.8174 -5 1 6 50.40 6.92 1.8107 -10 0 4 50.41 3.92 1.8104 -7 3 2 50.54 1.36 1.8061 0 4 1 50.93 4.74 1.7931 8 0 2 51.34 1.02 1.7796 3 3 3 51.95 4.64 1.7601 -9 1 5 52.07 4.63 1.7563 -1 1 6 52.14 15.68 1.7543 8 2 1 52.28 1.18 1.7500 5 3 2 52.33 4.10 1.7481 0 0 6 52.39 3.93 1.7464 2 4 1 52.46 2.29 1.7444 9 1 1 52.60 3.44 1.7401 -2 4 2 52.67 1.20 1.7379 -7 1 6 52.80 3.31 1.7339 1 3 4 52.90 4.34 1.7307 0 4 2 53.28 3.92 1.7194 4 2 4 53.60 6.54 1.7098 -4 4 1 53.76 10.65 1.7050 -8 2 5 53.88 1.51 1.7017 -10 0 5 54.02 1.97 1.6976 7 1 3 54.10 1.69 1.6951 6 2 3 54.61 9.19 1.6804 -4 2 6 54.78 2.53 1.6758 2 2 5 54.78 2.34 1.6757 -7 3 4 54.87 1.13 1.6732 -10 2 3 54.88 1.16 1.6729 -11 1 3 54.90 1.76 1.6724 -11 1 2 55.29 1.22 1.6614 4 0 5 55.50 7.47 1.6556 -2 2 6 55.72 2.37 1.6497 -2 4 3 55.72 3.03 1.6497 -10 2 1 55.88 5.65 1.6452 -6 2 6 56.36 10.19 1.6325 4 4 1 56.37 1.31 1.6323 -11 1 4 56.41 2.66 1.6311 -11 1 1 56.42 1.66 1.6307 10 0 1 56.51 1.32 1.6285 -1 3 5 56.69 8.16 1.6237 0 4 3 56.70 4.55 1.6236 -10 2 4 56.88 1.38 1.6188 -4 4 3 57.19 1.73 1.6107 -9 1 6 57.43 7.30 1.6047 -6 0 7 57.53 3.14 1.6020 8 0 3 57.77 1.46 1.5958 -9 3 2 58.35 2.59 1.5815 10 2 0 58.38 1.12 1.5808 -5 1 7 58.46 7.71 1.5787 -6 4 2 58.67 7.12 1.5736 -10 0 6 59.22 6.06 1.5602 -8 2 6 59.53 6.26 1.5530 6 4 0 59.88 8.51 1.5447 4 4 2 60.09 3.47 1.5397 -6 4 3 60.17 3.00 1.5380 -2 4 4 60.63 11.64 1.5274 -4 4 4 60.81 4.37 1.5233 9 3 0 61.24 13.43 1.5136 6 2 4 61.88 2.82 1.4994 10 0 2 61.93 2.99 1.4984 0 0 7 62.31 1.24 1.4900 10 2 1 62.40 1.51 1.4882 -5 3 6 63.09 1.36 1.4736 -6 4 4 63.38 3.21 1.4674 2 2 6 63.59 1.76 1.4631 11 1 1 63.66 2.12 1.4617 1 5 0 63.71 1.64 1.4607 12 0 0 63.93 2.48 1.4562 -9 3 5 64.03 2.53 1.4541 -1 3 6 64.04 1.10 1.4540 -1 5 1 64.17 3.41 1.4514 -2 2 7 64.23 12.96 1.4501 -12 2 3 64.25 6.64 1.4498 -8 4 2 64.37 1.30 1.4473 9 3 1 64.48 3.53 1.4451 4 0 6 64.56 1.28 1.4436 -12 2 2 64.65 3.41 1.4417 4 4 3 65.75 3.47 1.4202 -8 2 7 65.95 2.23 1.4165 -13 1 4 66.05 2.24 1.4145 -6 0 8 66.24 1.22 1.4109 -12 2 1 67.36 2.99 1.3902 -6 4 5 67.53 2.57 1.3871 0 2 7 67.65 5.38 1.3849 -12 2 5 67.90 6.76 1.3805 0 4 5 68.10 1.24 1.3768 -7 1 8 68.91 2.60 1.3626 -3 5 3 69.24 5.60 1.3570 12 2 0 69.25 4.09 1.3568 6 2 5 69.60 1.11 1.3508 8 4 1 69.82 2.36 1.3471 -14 0 4 70.13 2.84 1.3419 3 5 2 70.33 3.15 1.3385 -14 0 2 70.53 2.41 1.3353 8 2 4 70.56 2.34 1.3347 4 4 4 70.87 1.19 1.3296 -12 0 7 71.27 2.77 1.3232 6 4 3 71.30 3.17 1.3226 -12 2 6 71.53 3.12 1.3190 -14 0 5 71.58 6.84 1.3182 -4 2 8 71.85 2.45 1.3139 2 4 5 71.88 1.60 1.3135 5 3 5 71.93 1.46 1.3127 -10 4 3 71.93 1.98 1.3126 3 1 7 72.60 2.36 1.3021 -3 5 4 72.66 6.17 1.3013 -10 4 1 73.44 2.05 1.2894 8 0 5 73.51 3.47 1.2883 -10 4 4 73.52 1.56 1.2882 -7 5 2 73.76 1.15 1.2845 10 2 3 73.94 2.24 1.2819 8 4 2 74.30 2.03 1.2766 4 0 7 75.08 1.97 1.2652 0 4 6 75.63 1.17 1.2574 -14 2 2 75.93 1.47 1.2531 10 0 4 76.01 1.15 1.2520 14 0 0 76.35 1.02 1.2473 -10 4 5 76.84 1.83 1.2406 -10 2 8 78.50 1.42 1.2185 10 4 1 78.57 2.13 1.2175 -2 0 9 78.87 5.39 1.2136 12 2 2 79.35 5.28 1.2075 -6 4 7 79.44 2.82 1.2064 8 4 3 79.53 1.29 1.2052 -10 0 9 79.72 2.02 1.2029 -14 2 6 80.18 1.22 1.1971 -15 1 1 80.31 4.46 1.1955 2 6 1 80.42 5.25 1.1941 -10 4 6 80.48 4.07 1.1934 -2 6 2 80.68 1.77 1.1909 14 0 1 81.29 2.74 1.1835 -4 6 1 81.44 1.25 1.1818 1 5 5 81.73 4.03 1.1783 -8 2 9 82.16 3.22 1.1732 -12 2 8 82.34 1.00 1.1711 3 3 7 82.77 5.01 1.1660 2 2 8 83.24 2.16 1.1607 10 4 2 83.28 2.19 1.1602 0 4 7 83.70 1.05 1.1555 -2 2 9 83.85 1.03 1.1538 -14 2 7 84.01 1.22 1.1521 -4 6 3 85.19 1.21 1.1391 -6 6 1 85.42 1.37 1.1365 12 2 3 85.57 2.79 1.1349 4 4 6 85.68 1.24 1.1337 -10 4 7 86.27 1.46 1.1276 6 6 0 86.44 2.55 1.1258 2 6 3 86.75 1.44 1.1225 -6 6 3 87.00 1.42 1.1199 -6 4 8 87.95 2.50 1.1103 6 2 7 89.32 1.10 1.0968 -12 2 9 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.