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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060839
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.030
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    9.2860 9.547035   0  0  2    2    9.2949  9.537845    0.0089  0.009189
   18.6239 4.768124   0  0  4    2   18.6208  4.768923   -0.0031 -0.000799
   23.5636 3.777265  -1  1  3    2   23.5637  3.777253    0.0001  0.000012
   24.4794 3.637812   0  2  3    2   24.4764  3.638247   -0.0030 -0.000434
   26.3620 3.381839  -1  1  4    2   26.3484  3.383559   -0.0136 -0.001720
   28.0749 3.179053   0  0  6    2   28.0728  3.179282   -0.0021 -0.000229
   30.9159 2.892796   0  2  5    2   30.9183  2.892578    0.0024  0.000218
   32.2594 2.775208   1  1  5    2   32.2646  2.774772    0.0052  0.000435
   33.3185 2.689292  -1  1  6    2   33.3292  2.688451    0.0107  0.000841
   42.7986 2.112567   2  2  2    2   42.7976  2.112612   -0.0010 -0.000046
   47.6647 1.907489   0  0 10    2   47.6626  1.907569   -0.0021 -0.000080

 rmse = 0.00005235123
 
     A =5.114(1)               B =8.872(3)                C =19.164(2)           
 Alpha =90                  Beta =95.51(2)            Gamma =90                  
 
 Volume = 865.6(3)