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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060131
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.016
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   10.5546 8.387719   0  2  0    2   10.5280  8.408889   -0.0266 -0.021171
   19.0817 4.651163  -1  0  1    2   19.0815  4.651215   -0.0002 -0.000052
   21.1367 4.203020   0  4  0    2   21.1295  4.204445   -0.0072 -0.001425
   21.6052 4.112857   0 -4  1    2   21.6167  4.110685    0.0115  0.002172
   28.1363 3.170692   1 -4  1    2   28.1329  3.171070   -0.0034 -0.000378
   28.7372 3.105706   2  0  0    2   28.7407  3.105331    0.0035  0.000375
   30.4551 2.934227   0 -6  1    2   30.4637  2.933421    0.0086  0.000805
   34.3495 2.609785  -2  2  1    2   34.3496  2.609778    0.0001  0.000008
   36.5006 2.460697   1  0  2    2   36.4994  2.460776   -0.0012 -0.000079
   40.4816 2.227321   0 -8  1    2   40.4769  2.227568   -0.0047 -0.000246
   48.3999 1.879686  -3 -4  2    2   48.3992  1.879711   -0.0007 -0.000025
   50.8919 1.793307   0  8  1    2   50.8932  1.793264    0.0013  0.000043

 rmse = 0.00005495863
 
     A =6.358(1)               B =17.978(2)               C =6.258(2)            
 Alpha =110.41(1)           Beta =101.87(2)           Gamma =82.66(2)            
 
 Volume = 654.9(0)