Meneghinite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from the powder pattern of R050444 Euler R, Hellner E Zeitschrift fur Kristallographie 113 (1960) 345-372 Uber komplex zusammengesetzte sulfidische erze VI. Zur kristallstruktur des meneghinits, CuPb13Sb7S24 CELL PARAMETERS: 11.3567 24.0580 4.1274 90.000 90.000 90.000 SPACE GROUP: Pbnm ATOM X Y Z OCCUPANCY ISO(B) Cu 0.24000 0.25600 0.25000 0.250 0.700 Pb 0.15000 0.02600 0.25000 0.500 0.840 Sb 0.15000 0.02600 0.25000 0.500 0.840 Pb 0.34200 0.37400 0.75000 1.000 0.590 Pb 0.03600 0.43600 0.25000 0.500 0.700 Sb 0.03600 0.43600 0.25000 0.500 0.700 Pb 0.01500 0.28400 0.75000 1.000 0.800 Pb 0.22000 0.15100 0.75000 0.250 0.410 Sb 0.22000 0.15100 0.75000 0.750 0.410 S 0.47400 0.43700 0.25000 1.000 0.370 S 0.40600 0.11000 0.25000 1.000 0.410 S 0.08900 0.18300 0.25000 1.000 0.480 S 0.33600 0.23700 0.75000 1.000 0.140 S 0.16000 0.34800 0.25000 1.000 0.430 S 0.21700 0.47900 0.75000 1.000 0.280 X-RAY WAVELENGTHS: 1.540562 1.544390 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 10 +/- 22 +/- 3 MAX. ABS. INTENSITY / VOLUME**2: 71.94672260 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 10.70 / 10.73 2.51 / 1.25 8.2578 1 2 0 13.51 / 13.54 5.18 / 2.59 6.5508 1 3 0 14.72 / 14.75 1.20 / 0.60 6.0145 0 4 0 15.59 / 15.63 2.01 / 1.00 5.6783 2 0 0 16.67 / 16.71 2.18 / 1.09 5.3151 1 4 0 17.25 / 17.30 3.08 / 1.54 5.1350 2 2 0 20.03 / 20.08 5.32 / 2.66 4.4304 1 5 0 21.50 / 21.56 22.65 / 11.33 4.1289 2 4 0 22.76 / 22.82 3.83 / 1.92 3.9040 0 2 1 22.91 / 22.96 8.30 / 4.15 3.8792 1 0 1 23.51 / 23.57 9.52 / 4.76 3.7809 1 6 0 23.77 / 23.83 72.14 / 36.07 3.7396 3 1 0 24.09 / 24.15 25.41 / 12.70 3.6919 1 2 1 24.23 / 24.29 17.59 / 8.79 3.6709 2 5 0 24.63 / 24.70 11.54 / 5.77 3.6110 3 2 0 25.49 / 25.55 80.42 / 40.21 3.4921 1 3 1 26.01 / 26.07 6.62 / 3.31 3.4233 3 3 0 26.16 / 26.23 6.21 / 3.11 3.4031 0 4 1 26.94 / 27.01 3.01 / 1.50 3.3069 2 1 1 27.08 / 27.15 58.90 / 29.45 3.2895 1 7 0 27.20 / 27.27 31.88 / 15.94 3.2754 2 6 0 27.34 / 27.40 48.35 / 24.17 3.2599 1 4 1 28.94 / 29.02 44.60 / 22.30 3.0822 2 3 1 29.68 / 29.76 1.67 / 0.83 3.0073 0 8 0 30.01 / 30.09 1.32 / 0.66 2.9752 3 5 0 30.38 / 30.45 36.86 / 18.43 2.9402 2 7 0 30.60 / 30.68 100.00 / 50.00 2.9191 2 4 1 30.73 / 30.81 8.24 / 4.12 2.9071 1 8 0 31.07 / 31.15 1.52 / 0.76 2.8760 0 6 1 31.48 / 31.56 1.12 / 0.56 2.8392 4 0 0 31.71 / 31.79 3.64 / 1.82 2.8196 4 1 0 32.06 / 32.14 14.80 / 7.40 2.7898 3 0 1 32.08 / 32.16 1.45 / 0.73 2.7880 1 6 1 32.28 / 32.36 38.45 / 19.23 2.7713 3 1 1 32.37 / 32.45 7.35 / 3.67 2.7632 4 2 0 32.62 / 32.70 49.18 / 24.59 2.7430 2 5 1 32.93 / 33.01 10.30 / 5.15 2.7177 3 2 1 33.70 / 33.78 25.04 / 12.52 2.6576 2 8 0 34.00 / 34.08 3.15 / 1.58 2.6349 3 3 1 34.85 / 34.94 2.83 / 1.41 2.5725 1 7 1 34.92 / 35.01 2.60 / 1.30 2.5675 4 4 0 35.44 / 35.53 2.70 / 1.35 2.5308 3 4 1 36.95 / 37.05 3.05 / 1.53 2.4305 0 8 1 37.35 / 37.44 2.60 / 1.30 2.4058 0 10 0 37.53 / 37.62 5.50 / 2.75 2.3947 2 7 1 37.82 / 37.92 13.17 / 6.58 2.3767 1 8 1 38.83 / 38.93 2.35 / 1.18 2.3171 4 6 0 39.20 / 39.30 19.99 / 9.99 2.2962 4 2 1 39.31 / 39.41 2.40 / 1.20 2.2901 3 6 1 40.12 / 40.23 36.55 / 18.27 2.2456 4 3 1 40.33 / 40.44 4.08 / 2.04 2.2344 2 8 1 40.70 / 40.80 3.31 / 1.65 2.2152 2 10 0 40.97 / 41.07 5.40 / 2.70 2.2011 1 9 1 41.21 / 41.31 3.60 / 1.80 2.1889 4 7 0 41.31 / 41.42 3.13 / 1.57 2.1836 3 9 0 41.38 / 41.49 14.12 / 7.06 2.1801 4 4 1 41.66 / 41.77 1.59 / 0.79 2.1660 3 7 1 42.51 / 42.62 6.69 / 3.35 2.1249 5 4 0 43.50 / 43.62 38.59 / 19.30 2.0785 0 10 1 43.82 / 43.93 6.49 / 3.25 2.0645 4 8 0 43.83 / 43.95 46.41 / 23.20 2.0637 0 0 2 44.05 / 44.17 5.01 / 2.51 2.0540 5 5 0 44.25 / 44.36 1.83 / 0.91 2.0453 3 8 1 44.27 / 44.38 1.45 / 0.72 2.0445 1 10 1 44.82 / 44.94 6.14 / 3.07 2.0205 4 6 1 45.19 / 45.31 3.68 / 1.84 2.0048 0 12 0 45.71 / 45.83 5.59 / 2.79 1.9832 5 1 1 45.88 / 46.00 26.95 / 13.48 1.9763 5 6 0 46.49 / 46.61 2.76 / 1.38 1.9518 2 10 1 46.63 / 46.75 2.00 / 1.00 1.9462 4 9 0 46.95 / 47.07 5.50 / 2.75 1.9338 4 7 1 47.01 / 47.13 5.19 / 2.60 1.9314 5 3 1 47.04 / 47.17 8.23 / 4.11 1.9301 3 9 1 47.70 / 47.82 2.12 / 1.06 1.9052 1 11 1 47.97 / 48.10 8.03 / 4.02 1.8949 5 7 0 48.00 / 48.13 7.50 / 3.75 1.8938 3 11 0 48.03 / 48.15 6.48 / 3.24 1.8928 6 0 0 48.12 / 48.25 9.42 / 4.71 1.8892 5 4 1 48.19 / 48.31 5.50 / 2.75 1.8870 6 1 0 48.63 / 48.76 1.16 / 0.58 1.8707 1 5 2 49.31 / 49.44 15.08 / 7.54 1.8464 4 8 1 49.33 / 49.46 5.22 / 2.61 1.8460 2 4 2 49.80 / 49.93 2.11 / 1.06 1.8295 2 11 1 49.89 / 50.02 3.59 / 1.79 1.8265 1 13 0 50.02 / 50.15 3.00 / 1.50 1.8219 3 10 1 50.33 / 50.46 2.40 / 1.20 1.8114 1 6 2 50.47 / 50.60 18.86 / 9.43 1.8068 3 1 2 50.57 / 50.71 12.57 / 6.29 1.8033 0 12 1 50.71 / 50.84 4.92 / 2.46 1.7989 2 5 2 50.92 / 51.06 3.32 / 1.66 1.7917 3 2 2 51.21 / 51.34 10.22 / 5.11 1.7825 5 6 1 51.54 / 51.68 7.09 / 3.55 1.7717 3 12 0 51.68 / 51.81 2.09 / 1.05 1.7674 3 3 2 51.90 / 52.04 1.33 / 0.66 1.7603 4 9 1 51.92 / 52.06 1.47 / 0.74 1.7595 2 13 0 52.29 / 52.43 18.80 / 9.40 1.7482 1 7 2 52.36 / 52.50 9.71 / 4.86 1.7460 2 6 2 53.14 / 53.28 1.71 / 0.86 1.7221 5 7 1 53.17 / 53.31 22.39 / 11.20 1.7212 3 11 1 53.25 / 53.39 1.58 / 0.79 1.7188 2 12 1 53.26 / 53.41 1.97 / 0.98 1.7184 0 14 0 53.34 / 53.48 2.80 / 1.40 1.7161 6 1 1 53.78 / 53.92 5.04 / 2.52 1.7032 6 2 1 53.92 / 54.06 4.92 / 2.46 1.6991 1 14 0 54.26 / 54.41 13.03 / 6.52 1.6892 2 7 2 54.48 / 54.63 3.30 / 1.65 1.6828 1 8 2 55.10 / 55.25 1.47 / 0.73 1.6653 4 1 2 55.53 / 55.68 3.13 / 1.57 1.6535 4 2 2 55.85 / 56.00 2.41 / 1.21 1.6448 2 14 0 56.40 / 56.56 10.54 / 5.27 1.6300 2 8 2 56.83 / 56.98 1.19 / 0.59 1.6187 7 1 0 57.22 / 57.38 1.16 / 0.58 1.6085 4 4 2 57.25 / 57.41 5.22 / 2.61 1.6078 7 2 0 57.65 / 57.81 1.45 / 0.73 1.5976 4 11 1 57.95 / 58.10 3.34 / 1.67 1.5902 7 3 0 58.72 / 58.88 2.57 / 1.28 1.5712 1 14 1 58.91 / 59.07 1.28 / 0.64 1.5664 0 10 2 59.58 / 59.75 3.50 / 1.75 1.5503 4 13 0 59.88 / 60.04 3.38 / 1.69 1.5435 2 15 0 59.98 / 60.14 1.19 / 0.59 1.5411 4 6 2 60.55 / 60.71 4.13 / 2.07 1.5279 2 14 1 61.34 / 61.51 1.85 / 0.93 1.5100 2 10 2 61.73 / 61.90 2.07 / 1.04 1.5016 4 7 2 61.80 / 61.97 1.81 / 0.90 1.4998 3 9 2 61.88 / 62.05 5.75 / 2.88 1.4982 7 2 1 62.55 / 62.72 7.03 / 3.51 1.4839 7 3 1 62.62 / 62.80 3.82 / 1.91 1.4822 1 15 1 62.71 / 62.88 3.88 / 1.94 1.4804 5 4 2 63.20 / 63.37 5.04 / 2.52 1.4701 4 14 0 63.34 / 63.52 1.12 / 0.56 1.4671 7 7 0 63.71 / 63.89 4.03 / 2.01 1.4595 4 8 2 63.89 / 64.07 3.05 / 1.53 1.4558 5 5 2 64.34 / 64.52 5.94 / 2.97 1.4467 6 9 1 64.39 / 64.57 4.96 / 2.48 1.4457 2 15 1 64.64 / 64.82 2.39 / 1.20 1.4407 7 5 1 64.78 / 64.96 2.40 / 1.20 1.4380 0 12 2 65.32 / 65.50 17.57 / 8.79 1.4273 5 6 2 65.92 / 66.10 1.29 / 0.64 1.4159 4 9 2 66.79 / 66.98 10.11 / 5.06 1.3995 6 10 1 66.95 / 67.14 1.44 / 0.72 1.3965 4 15 0 66.99 / 67.18 5.58 / 2.79 1.3958 5 7 2 67.02 / 67.20 5.24 / 2.62 1.3953 3 11 2 67.04 / 67.23 4.50 / 2.25 1.3949 6 0 2 67.16 / 67.35 3.84 / 1.92 1.3926 6 1 2 68.07 / 68.26 2.98 / 1.49 1.3763 6 12 0 68.55 / 68.75 2.59 / 1.29 1.3677 1 13 2 68.91 / 69.10 4.91 / 2.45 1.3616 8 5 0 69.17 / 69.36 1.22 / 0.61 1.3571 1 2 3 69.62 / 69.82 3.40 / 1.70 1.3494 7 8 1 69.79 / 69.99 4.48 / 2.24 1.3464 1 3 3 69.92 / 70.12 5.32 / 2.66 1.3443 3 12 2 70.24 / 70.44 1.12 / 0.56 1.3389 2 13 2 70.67 / 70.87 3.17 / 1.58 1.3319 1 4 3 70.82 / 71.02 5.76 / 2.88 1.3295 1 17 1 70.94 / 71.15 1.29 / 0.65 1.3274 1 18 0 71.20 / 71.40 1.95 / 0.98 1.3232 6 13 0 71.37 / 71.57 1.56 / 0.78 1.3205 0 14 2 71.47 / 71.67 2.98 / 1.49 1.3189 2 3 3 71.73 / 71.94 8.76 / 4.38 1.3147 7 9 1 71.92 / 72.13 3.95 / 1.98 1.3117 1 14 2 72.33 / 72.54 7.28 / 3.64 1.3052 2 4 3 72.48 / 72.69 1.81 / 0.91 1.3030 2 17 1 72.61 / 72.82 2.36 / 1.18 1.3010 2 18 0 73.13 / 73.34 1.14 / 0.57 1.2931 3 0 3 73.13 / 73.34 4.05 / 2.02 1.2930 8 5 1 73.25 / 73.46 3.15 / 1.58 1.2912 3 1 3 73.44 / 73.65 4.07 / 2.03 1.2883 2 5 3 73.58 / 73.79 1.96 / 0.98 1.2862 2 14 2 74.07 / 74.28 1.74 / 0.87 1.2789 7 10 1 74.47 / 74.69 1.43 / 0.71 1.2730 8 6 1 74.79 / 75.01 4.49 / 2.25 1.2683 7 2 2 75.29 / 75.51 1.26 / 0.63 1.2612 7 12 0 75.40 / 75.62 2.87 / 1.44 1.2596 7 3 2 75.48 / 75.70 2.13 / 1.06 1.2584 1 19 0 75.73 / 75.95 1.44 / 0.72 1.2550 9 2 0 76.17 / 76.40 3.62 / 1.81 1.2488 5 15 1 76.55 / 76.77 1.56 / 0.78 1.2436 1 8 3 76.75 / 76.97 6.59 / 3.30 1.2408 2 18 1 76.84 / 77.07 3.12 / 1.56 1.2395 4 13 2 77.10 / 77.33 3.07 / 1.53 1.2360 2 15 2 77.43 / 77.66 2.45 / 1.22 1.2316 4 2 3 78.03 / 78.26 4.62 / 2.31 1.2236 4 3 3 78.31 / 78.54 2.19 / 1.10 1.2200 7 13 0 78.87 / 79.10 1.84 / 0.92 1.2127 4 4 3 79.13 / 79.37 1.10 / 0.55 1.2093 4 18 0 79.38 / 79.62 1.36 / 0.68 1.2061 7 12 1 79.45 / 79.69 5.64 / 2.82 1.2052 9 1 1 79.81 / 80.05 3.66 / 1.83 1.2007 9 2 1 79.89 / 80.13 13.01 / 6.50 1.1997 5 16 1 80.08 / 80.32 4.85 / 2.43 1.1974 4 14 2 80.21 / 80.45 1.07 / 0.54 1.1958 7 7 2 80.33 / 80.57 5.70 / 2.85 1.1943 0 10 3 81.25 / 81.50 1.03 / 0.52 1.1830 4 6 3 82.87 / 83.12 1.40 / 0.70 1.1640 3 9 3 83.17 / 83.43 1.91 / 0.95 1.1605 4 18 1 83.52 / 83.78 1.52 / 0.76 1.1565 4 15 2 83.53 / 83.79 1.05 / 0.52 1.1564 4 19 0 83.67 / 83.93 1.71 / 0.85 1.1549 5 4 3 84.55 / 84.81 3.15 / 1.57 1.1450 6 12 2 84.57 / 84.83 2.83 / 1.41 1.1449 4 8 3 84.91 / 85.17 2.12 / 1.06 1.1411 9 9 0 85.34 / 85.60 5.25 / 2.63 1.1365 8 5 2 85.53 / 85.80 1.57 / 0.79 1.1344 10 1 0 85.54 / 85.80 2.49 / 1.25 1.1344 0 12 3 86.03 / 86.30 2.06 / 1.03 1.1291 5 6 3 87.26 / 87.53 1.46 / 0.73 1.1164 1 18 2 87.50 / 87.77 2.17 / 1.08 1.1139 6 13 2 87.58 / 87.86 4.86 / 2.43 1.1131 3 11 3 88.07 / 88.35 1.15 / 0.58 1.1081 6 2 3 88.84 / 89.12 2.72 / 1.36 1.1006 2 18 2 88.91 / 89.19 2.09 / 1.05 1.0998 9 9 1 89.25 / 89.53 2.33 / 1.16 1.0965 3 21 0 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.