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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050193
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.071
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   19.3771 4.593761   0  2  1    2   19.3872  4.591390    0.0101  0.002371
   21.0438 4.232305  -2  0  1    2   21.0486  4.231356    0.0048  0.000949
   23.1154 3.856306   2  0  0    2   23.1132  3.856672   -0.0022 -0.000366
   41.2359 2.191079   1 -5  1    2   41.2432  2.190709    0.0073  0.000370
   41.8091 2.162304   0  6  0    2   41.8078  2.162369   -0.0013 -0.000065
   47.1690 1.927960   4  0  0    2   47.1593  1.928336   -0.0097 -0.000375
   55.0859 1.667772  -3  5  3    2   55.0824  1.667870   -0.0035 -0.000099
   65.2750 1.429627  -6  0  2    2   65.2773  1.429582    0.0023  0.000045
   66.4038 1.408009   4  0  2    2   66.4064  1.407960    0.0026  0.000050
   74.2385 1.277456  -4  8  2    2   74.2402  1.277431    0.0017  0.000026
   74.6248 1.271791   2 -8  2    2   74.6226  1.271823   -0.0022 -0.000032

 rmse = 0.00007051960
 
     A =8.5886(6)              B =12.976(2)               C =7.224(2)            
 Alpha =90.33(1)            Beta =116.08(1)           Gamma =89.07(2)            
 
 Volume = 723.0(0)