Minium Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from the powder pattern for R050426 Gavarri J R, Weigel D Journal of Solid State Chemistry 13 (1975) 252-257 Oxydes de plomb. I. structure cristalline du minium Pb3O4, a temperature ambiante (293 K) Locality: synthetic Sample: T = 293 K CELL PARAMETERS: 8.811978 8.811978 6.564547 90.00000 90.00000 90.00000 SPACE GROUP: P4_2/mbc ATOM X Y Z OCCUPANCY ISO(B) Pb 0.00000 0.50000 0.25000 1.000 1.500 Pb 0.14000 0.16300 0.00000 1.000 1.500 O 0.67100 0.17100 0.25000 1.000 1.000 O 0.09600 0.63700 0.00000 1.000 1.000 X-RAY WAVELENGTH: 1.541838 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 8 +/- 8 +/- 6 MAX. ABS. INTENSITY / VOLUME**2: 407.8898772 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 14.22 11.02 6.2310 1 1 0 20.15 1.56 4.4060 2 0 0 24.32 2.72 3.6584 2 0 1 26.37 100.00 3.3788 2 1 1 27.16 5.08 3.2823 0 0 2 28.64 13.05 3.1155 2 2 0 30.78 37.73 2.9040 1 1 2 32.11 48.73 2.7866 3 1 0 34.05 26.06 2.6322 2 0 2 36.76 2.13 2.4440 3 2 0 39.32 4.12 2.2904 3 2 1 39.88 5.43 2.2597 2 2 2 40.95 1.60 2.2030 4 0 0 44.56 9.78 2.0322 4 1 1 46.04 10.73 1.9704 4 2 0 46.29 1.84 1.9603 3 2 2 47.50 18.43 1.9131 2 1 3 49.82 22.80 1.8292 4 0 2 50.96 1.05 1.7910 4 1 2 52.08 24.35 1.7551 3 3 2 52.95 2.18 1.7282 5 1 0 53.83 1.14 1.7021 4 3 1 54.27 1.35 1.6894 4 2 2 56.00 6.22 1.6411 0 0 4 56.41 1.26 1.6302 3 2 3 58.06 11.57 1.5878 5 2 1 59.29 4.57 1.5578 4 4 0 60.51 5.07 1.5292 5 1 2 60.52 3.46 1.5289 4 1 3 61.30 1.77 1.5112 5 3 0 63.09 1.13 1.4727 5 3 1 63.28 5.22 1.4687 6 0 0 64.09 2.10 1.4520 2 2 4 66.00 1.83 1.4146 6 1 1 66.02 10.18 1.4141 3 1 4 68.28 1.58 1.3727 5 3 2 69.78 2.83 1.3469 5 4 1 72.02 5.45 1.3105 5 2 3 73.84 3.20 1.2825 6 2 2 75.31 3.94 1.2610 4 2 4 76.41 3.59 1.2456 2 1 5 80.69 1.03 1.1900 5 1 4 82.79 4.40 1.1651 7 1 2 82.80 1.59 1.1650 5 4 3 83.49 3.73 1.1571 7 3 0 84.55 5.27 1.1452 6 4 2 85.98 2.55 1.1298 4 4 4 87.05 1.00 1.1187 4 1 5 87.73 1.07 1.1117 5 3 4 89.48 3.30 1.0944 6 0 4 89.48 3.30 1.0944 6 0 4 XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.