******************************************************************************
       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 R060089
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.049
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   20.1695 4.409479   2  1  1    2   20.1745  4.408397    0.0050  0.001082
   13.7966 6.435808  -1  1  1    2   13.8016  6.433494    0.0050  0.002313
   26.9190 3.315234   1  3  2    2   26.9228  3.314778    0.0038  0.000456
   19.3099 4.604283  -2  1  1    2   19.3123  4.603713    0.0024  0.000571
   10.7962 8.224797   0  0  1    2   10.7985  8.223027    0.0023  0.001770
   30.8501 2.900491   2  6  0    2   30.8509  2.900416    0.0008  0.000075
   20.5445 4.329640   0  4  1    2   20.5444  4.329656   -0.0001 -0.000015
   22.9563 3.878965  -2  3  1    2   22.9562  3.878977   -0.0001 -0.000012
   18.8096 4.725922  -2  0  1    2   18.8094  4.725979   -0.0002 -0.000056
   28.4662 3.138154   0  6  1    2   28.4657  3.138206   -0.0005 -0.000052
   19.6936 4.515211   2  0  1    2   19.6928  4.515395   -0.0008 -0.000184
   15.9206 5.579025   2  0  0    2   15.9188  5.579643   -0.0018 -0.000617
   21.6470 4.111059   0  0  2    2   21.6446  4.111514   -0.0024 -0.000455
    8.725410.182509   0  2  0    2    8.7228 10.185536   -0.0026 -0.003027
   27.1749 3.284537   3  1  1    2   27.1722  3.284860   -0.0027 -0.000323
   23.3640 3.812051   0  2  2    2   23.3605  3.812611   -0.0035 -0.000561
   17.4508 5.091749   0  4  0    2   17.4473  5.092768   -0.0035 -0.001019

 rmse = 0.00001530086
 
     A =11.1727(9)             B =20.371(1)               C =8.2329(6)           
 Alpha =90                  Beta =92.810(7)           Gamma =90                  
 
 Volume = 1871.6(2)