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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070480
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.016
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   12.6628 6.976157   1  1  0    2   12.6586  6.978446   -0.0042 -0.002289
   14.3786 6.148234   0  2  0    2   14.3789  6.148107    0.0003  0.000126
   16.8025 5.267196  -1  1  1    2   16.8007  5.267764   -0.0018 -0.000568
   20.9234 4.238975   2  0  0    2   20.9292  4.237816    0.0058  0.001159
   25.1520 3.535521   0  0  2    2   25.1479  3.536084   -0.0041 -0.000563
   27.1773 3.276624  -2  2  1    2   27.1783  3.276508    0.0010  0.000116
   27.8778 3.195908   1  3  1    2   27.8813  3.195514    0.0035  0.000394
   29.0120 3.073563   0  4  0    2   29.0073  3.074054   -0.0047 -0.000491
   29.5158 3.022265   1  1  2    2   29.5175  3.022098    0.0017  0.000167
   31.6953 2.819340   0  4  1    2   31.6965  2.819239    0.0012  0.000101
   32.4757 2.753384   3  1  0    2   32.4747  2.753466   -0.0010 -0.000083
   37.2999 2.407758  -2  4  1    2   37.3023  2.407608    0.0024  0.000150
   38.6623 2.326025   3  3  0    2   38.6602  2.326149   -0.0021 -0.000124

 rmse = 0.00002292968
 
     A =8.5535(6)              B =12.2962(8)              C =7.1371(8)           
 Alpha =90                  Beta =97.74(1)            Gamma =90                  
 
 Volume = 743.82(8)