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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R040108
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.058
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    8.9271 9.961961   0  0  2    2    8.9397  9.947908    0.0126  0.014053
   17.8784 4.973141   0  0  4    2   17.8755  4.973954   -0.0029 -0.000813
   22.9038 3.889305  -1  1  3    2   22.9080  3.888606    0.0042  0.000699
   23.8259 3.740463   0  2  3    2   23.8269  3.740311    0.0010  0.000152
   25.5300 3.493955  -1  1  4    2   25.5217  3.495076   -0.0083 -0.001121
   26.9234 3.315818   0  0  6    2   26.9222  3.315969   -0.0012 -0.000151
   27.8792 3.204037   1  1  4    2   27.8904  3.202778    0.0112  0.001258
   29.9223 2.989329   0  2  5    2   29.9215  2.989406   -0.0008 -0.000077
   31.3048 2.860148   1  1  5    2   31.2961  2.860927   -0.0087 -0.000779
   32.1108 2.790043  -1  1  6    2   32.1132  2.789839    0.0024  0.000204
   45.6124 1.989616   0  0 10    2   45.6132  1.989582    0.0008  0.000035

 rmse = 0.00004654512
 
     A =     5.220(2)          B =     9.058(3)           C =    19.997(2)       
 Alpha =    90.             Beta =    95.79(1)        Gamma =    90.             
 
 Volume =    940.9(4)