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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050289
 
 Symmetry constraint is: HEXAGONAL   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.036
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   17.6206 5.039453   0  1  2    2   17.6288  5.037117    0.0082  0.002336
   24.3432 3.658766   1  1  0    2   24.3497  3.657801    0.0065  0.000965
   28.7009 3.111682   0  2  1    2   28.7011  3.111664    0.0002  0.000018
   29.2738 3.051999   1  1  3    2   29.2747  3.051905    0.0009  0.000094
   32.3478 2.768315   0  0  6    2   32.3482  2.768283    0.0004  0.000032
   35.6590 2.518216   0  2  4    2   35.6540  2.518558   -0.0050 -0.000342
   40.6069 2.221785   1  0  7    2   40.6013  2.222080   -0.0056 -0.000295
   45.9896 1.973280   0  3  3    2   45.9924  1.973165    0.0028  0.000115
   47.9049 1.898700   0  2  7    2   47.8938  1.899113   -0.0111 -0.000413
   49.3718 1.845624   0  0  9    2   49.3747  1.845522    0.0029  0.000102
   49.8510 1.828986   2  2  0    2   49.8535  1.828900    0.0025  0.000086
   52.6955 1.736690   2  0  8    2   52.7026  1.736472    0.0071  0.000218
   60.6740 1.525879   2  2  6    2   60.6708  1.525953   -0.0032 -0.000074
   63.1878 1.471054   0  2 10    2   63.1895  1.471020    0.0017  0.000035

 rmse = 0.00005329120
 
     A =7.3156(4)              B =7.3156(4)               C =16.6097(8)          
 Alpha =90                  Beta =90                  Gamma =120                 
 
 Volume = 769.83(8)