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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050639
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.001
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   14.6052 6.059510   0  0  2    2   14.6051  6.059534   -0.0001 -0.000024
   18.0814 4.901699   0  1  1    2   18.0707  4.904586   -0.0107 -0.002887
   21.4457 4.139780  -1  1  1    2   21.4457  4.139780    0.0000  0.000000
   23.0828 3.849758   2  0  0    2   23.0818  3.849927   -0.0010 -0.000169
   27.6076 3.228236   0  1  3    2   27.6201  3.226802    0.0125  0.001434
   34.2155 2.618409   0  2  1    2   34.2159  2.618376    0.0004  0.000033
   44.8376 2.019706   0  0  6    2   44.8343  2.019845   -0.0033 -0.000139
   47.1743 1.924969   4  0  0    2   47.1744  1.924963    0.0001  0.000005
   48.0998 1.890070   0  1  6    2   48.0950  1.890246   -0.0048 -0.000176
   50.7246 1.798253   0  2  5    2   50.7269  1.798178    0.0023  0.000075
   53.3866 1.714695   0  3  2    2   53.3853  1.714734   -0.0013 -0.000039
   55.7429 1.647667   0  1  7    2   55.7459  1.647585    0.0030  0.000082

 rmse = 0.00004450186
 
     A =7.6999(6)              B =5.3634(3)               C =12.1192(6)          
 Alpha =90                  Beta =90.2(1)             Gamma =90                  
 
 Volume = 500.49(5)