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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050144
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.007
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   16.1446 5.487660   1  1  1    2   16.1438  5.487935   -0.0008 -0.000275
   17.1252 5.175457   0  0  2    2   17.1087  5.180416   -0.0165 -0.004959
   21.5791 4.115935   2  1  0    2   21.5869  4.114467    0.0078  0.001469
   21.9570 4.045922   1  1  2    2   21.9681  4.043908    0.0111  0.002014
   23.2528 3.823241   2  1  1    2   23.2483  3.823976   -0.0045 -0.000735
   25.8264 3.447697   2  0  2    2   25.8334  3.446778    0.0070  0.000919
   27.8585 3.200594   1  2  2    2   27.8600  3.200423    0.0015  0.000171
   31.8706 2.806157   3  1  1    2   31.8748  2.805794    0.0042  0.000363
   34.6130 2.589801   0  0  4    2   34.6074  2.590208   -0.0056 -0.000407
   36.3084 2.472644   3  2  1    2   36.3021  2.473059   -0.0063 -0.000414
   37.3638 2.405177   1  1  4    2   37.3719  2.404671    0.0081  0.000506
   38.0925 2.360817   2  2  3    2   38.0891  2.361017   -0.0034 -0.000200
   47.5263 1.911820   4  2  2    2   47.5219  1.911988   -0.0044 -0.000167
   48.4472 1.877605   4  1  3    2   48.4461  1.877646   -0.0011 -0.000041
   59.2629 1.558108   5  3  1    2   59.2658  1.558040    0.0029  0.000068

 rmse = 0.00004970883
 
     A =9.234(1)               B =9.068(3)                C =10.361(1)           
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 867.6(0)