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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060977XrayPowderProfile
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.128
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    8.565210.163292   0  0  2    2    8.5463 10.185340   -0.0189 -0.022049
   17.3039 5.083130   0  0  4    2   17.2710  5.092670   -0.0329 -0.009540
   18.6813 4.713886   3  1  0    2   18.6794  4.714354   -0.0019 -0.000468
   20.6017 4.281326   3  1  2    2   20.6166  4.278293    0.0149  0.003032
   25.0374 3.535843   5  1  1    2   25.0631  3.532291    0.0257  0.003552
   26.1460 3.389113   0  0  6    2   26.0987  3.395113   -0.0473 -0.006000
   27.0627 3.276899   4  0  5    2   27.0422  3.279321   -0.0205 -0.002422
   27.9800 3.172008   5  1  3    2   27.9855  3.171397    0.0055  0.000611
   32.4985 2.742293   8  0  1    2   32.5497  2.738114    0.0512  0.004178
   34.4164 2.594305   7  1  3    2   34.4117  2.594645   -0.0047 -0.000341
   34.8784 2.561117   2  1  7    2   34.9245  2.557852    0.0461  0.003265
   35.8268 2.495706   8  1  1    2   35.7581  2.500328   -0.0687 -0.004622
   37.7258 2.374755   4  2  4    2   37.7572  2.372860    0.0314  0.001895
   39.2248 2.287681   8  0  5    2   39.2399  2.286838    0.0151  0.000843
   42.8424 2.103090   4  2  6    2   42.8135  2.104438   -0.0289 -0.001348

 rmse = 0.00029203317
 
     A =22.11(1)               B =6.134(7)                C =20.37(2)            
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 2760(3)