Owyheeite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from single crystal data of R070543 Laufek F, Pazout R, Makovicky E European Journal of Mineralogy 19 (2007) 557-566 Crystal structure of owyheeite, Ag1.5Pb4.43Sb6.07S14: refinement from powder synchrotron X-ray diffraction Locality: Kutna Hora, central Bohemia, Czech Republic _database_code_amcsd 0007225 CELL PARAMETERS: 4.0700 27.1500 22.7400 90.000 90.020 90.000 SPACE GROUP: P2_1/c ATOM X Y Z OCCUPANCY ISO(B) Ag 0.73520 0.16620 0.05900 1.000 3.869 Pb 0.27360 0.86100 0.36660 1.000 3.948 Pb 0.73060 0.21520 0.47500 1.000 3.948 Pb 0.72650 0.29890 0.31690 1.000 3.948 Pb 0.28960 0.95900 0.21290 1.000 3.948 Pb 0.22490 0.07680 0.48820 0.430 3.948 Sb 0.22490 0.07680 0.48820 0.570 3.948 Sb 0.75970 0.00560 0.36560 1.000 3.806 Sb 0.23110 0.15810 0.33530 0.500 3.806 Ag 0.23110 0.15810 0.33530 0.500 3.806 Sb 0.22110 0.22770 0.17210 1.000 3.806 Sb 0.20960 0.10740 0.93770 1.000 3.806 Sb 0.79720 0.03790 0.07560 1.000 3.806 Sb 0.32080 0.10370 0.20260 1.000 3.806 S 0.21740 0.23650 0.38040 1.000 3.490 S 0.21020 0.15680 0.54350 1.000 3.490 S 0.73520 0.92870 0.31030 1.000 3.490 S 0.74720 0.03860 0.18260 1.000 3.490 S 0.19160 0.12680 0.83380 1.000 3.490 S 0.26490 0.30850 0.22010 1.000 3.490 S 0.73030 0.25690 0.09910 1.000 3.490 S 0.75760 0.04480 0.55580 1.000 3.490 S 0.68470 0.12350 0.40940 1.000 3.490 S 0.27130 0.03610 0.30410 1.000 3.490 S 0.23490 0.97410 0.07650 1.000 3.490 S 0.78580 0.17020 0.95390 1.000 3.490 S 0.24370 0.11410 0.09230 1.000 3.490 S 0.75510 0.18460 0.25650 1.000 3.490 X-RAY WAVELENGTH: 1.541838 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 3 +/- 24 +/- 20 MAX. ABS. INTENSITY / VOLUME**2: 36.80615116 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 5.07 4.75 17.4330 0 1 1 6.51 2.98 13.5750 0 2 0 7.58 12.27 11.6560 0 2 1 10.15 2.60 8.7165 0 2 2 10.52 4.53 8.4086 0 3 1 12.12 8.05 7.3008 0 1 3 12.50 6.58 7.0808 0 3 2 15.20 5.03 5.8280 0 4 2 18.10 1.69 4.8999 0 5 2 19.62 1.45 4.5250 0 6 0 19.79 1.43 4.4855 0 1 5 20.01 2.83 4.4380 0 6 1 20.12 5.02 4.4142 0 5 3 20.38 1.78 4.3582 0 4 4 20.60 6.03 4.3124 0 2 5 21.13 4.26 4.2043 0 6 2 22.08 12.68 4.0250 1 1 0 22.43 12.97 3.9637 -1 1 1 22.43 8.43 3.9632 1 1 1 22.89 46.93 3.8853 0 6 3 23.21 1.56 3.8323 -1 0 2 23.22 1.48 3.8315 1 0 2 23.44 3.39 3.7947 -1 1 2 23.45 5.97 3.7939 1 1 2 23.47 10.61 3.7900 0 0 6 23.55 8.60 3.7782 0 4 5 23.70 14.01 3.7536 0 1 6 23.97 8.77 3.7119 1 3 0 24.14 3.04 3.6874 1 2 2 24.25 3.29 3.6709 0 7 2 24.29 11.81 3.6636 -1 3 1 24.30 9.05 3.6632 1 3 1 24.38 14.66 3.6504 0 2 6 25.05 11.73 3.5554 -1 1 3 25.05 19.60 3.5544 1 1 3 25.15 13.83 3.5404 0 6 4 25.24 16.31 3.5290 -1 3 2 25.24 7.93 3.5283 1 3 2 25.55 1.84 3.4866 0 5 5 25.80 100.00 3.4528 0 7 3 25.82 2.21 3.4503 -1 4 1 25.82 4.03 3.4500 1 4 1 26.56 1.50 3.3566 0 8 1 26.71 20.04 3.3371 -1 4 2 26.72 27.51 3.3366 1 4 2 26.74 1.05 3.3341 -1 3 3 26.75 1.16 3.3332 1 3 3 26.94 22.12 3.3099 -1 0 4 26.95 16.28 3.3088 1 0 4 27.39 1.96 3.2567 1 5 0 27.66 76.84 3.2256 0 1 7 27.74 1.41 3.2157 -1 2 4 27.85 60.21 3.2039 0 7 4 28.14 5.70 3.1709 -1 4 3 28.15 2.98 3.1702 1 4 3 28.51 3.84 3.1306 1 5 2 28.72 9.48 3.1085 -1 3 4 28.73 1.05 3.1078 0 5 6 28.73 16.78 3.1076 1 3 4 28.82 1.36 3.0975 0 8 3 29.63 7.04 3.0147 -1 1 5 29.78 15.80 2.9997 -1 6 1 29.79 2.16 2.9995 1 6 1 29.86 2.68 2.9919 1 5 3 30.04 4.53 2.9750 -1 4 4 30.19 6.12 2.9604 -1 2 5 30.20 14.51 2.9594 1 2 5 30.29 1.55 2.9511 0 7 5 30.57 1.51 2.9244 -1 6 2 30.66 5.56 2.9158 0 9 2 30.68 26.75 2.9140 0 8 4 31.10 43.96 2.8761 -1 3 5 31.11 44.30 2.8753 1 3 5 31.47 7.16 2.8425 0 0 8 31.65 4.71 2.8270 0 1 8 31.67 2.95 2.8255 1 5 4 31.84 24.89 2.8106 -1 6 3 31.85 20.92 2.8101 1 6 3 31.87 46.20 2.8078 1 7 0 31.93 6.80 2.8029 0 9 3 32.12 1.61 2.7866 1 7 1 32.27 7.16 2.7741 -1 0 6 32.28 8.62 2.7732 1 0 6 32.33 5.11 2.7694 -1 4 5 32.86 1.32 2.7258 1 7 2 32.96 10.62 2.7180 -1 2 6 32.97 8.88 2.7170 1 2 6 33.55 3.48 2.6715 -1 6 4 33.55 3.09 2.6709 1 6 4 33.63 3.29 2.6647 0 9 4 33.79 6.09 2.6523 -1 3 6 33.81 2.61 2.6515 1 3 6 33.86 3.84 2.6475 1 5 5 34.64 14.88 2.5896 -1 8 1 34.64 7.02 2.5895 1 8 1 35.33 1.42 2.5407 -1 8 2 35.67 1.54 2.5172 1 7 4 35.69 1.58 2.5158 0 1 9 35.72 2.28 2.5139 0 9 5 35.98 1.58 2.4961 -1 2 7 36.38 2.39 2.4697 1 5 6 36.68 1.71 2.4500 0 10 4 36.94 5.01 2.4336 0 3 9 37.10 5.95 2.4235 1 9 0 37.28 3.25 2.4120 0 11 2 37.84 1.27 2.3777 1 4 7 37.97 2.32 2.3695 -1 8 4 37.98 2.18 2.3691 1 8 4 38.35 1.25 2.3469 0 11 3 39.16 1.16 2.3003 -1 5 7 39.17 1.15 2.2996 1 5 7 39.22 4.87 2.2972 -1 2 8 39.23 5.41 2.2964 1 2 8 39.84 2.81 2.2625 0 12 0 39.86 3.01 2.2617 -1 8 5 39.87 1.41 2.2612 1 8 5 39.97 2.58 2.2559 1 7 6 40.12 10.55 2.2476 -1 10 1 40.12 12.83 2.2475 1 10 1 40.21 1.27 2.2428 0 2 10 40.66 2.01 2.2190 0 12 2 40.73 12.35 2.2154 -1 10 2 40.73 11.14 2.2152 1 10 2 40.74 6.29 2.2145 -1 6 7 40.76 9.26 2.2139 1 6 7 40.91 11.60 2.2061 0 6 9 40.94 8.39 2.2044 -1 4 8 40.95 7.48 2.2038 1 4 8 41.44 2.41 2.1791 0 8 8 41.63 1.26 2.1693 0 11 5 41.90 1.04 2.1562 0 4 10 42.19 3.17 2.1418 -1 5 8 42.20 2.74 2.1412 1 5 8 42.71 1.45 2.1171 0 7 9 42.85 4.65 2.1104 1 11 0 43.04 6.45 2.1014 -1 11 1 43.04 2.88 2.1014 1 11 1 43.09 1.27 2.0991 -1 10 4 43.13 15.64 2.0975 0 5 10 43.52 9.90 2.0797 0 13 1 43.76 3.74 2.0688 0 9 8 43.77 1.46 2.0683 0 11 6 44.25 6.49 2.0470 -1 4 9 44.26 4.89 2.0464 1 4 9 44.37 2.81 2.0416 1 9 6 44.52 42.94 2.0350 2 0 0 44.56 8.19 2.0332 -1 8 7 44.57 7.63 2.0328 1 8 7 44.60 5.28 2.0319 0 6 10 44.65 1.62 2.0293 2 1 0 44.72 4.05 2.0267 0 8 9 44.84 1.83 2.0212 2 1 1 45.03 1.55 2.0134 0 13 3 45.40 8.16 1.9978 -1 7 8 45.41 3.98 1.9973 1 7 8 45.43 5.21 1.9966 -1 5 9 45.44 7.85 1.9960 1 5 9 45.71 1.46 1.9849 1 0 10 46.21 1.42 1.9646 -1 2 10 46.22 1.97 1.9640 1 2 10 46.85 1.72 1.9392 1 6 9 46.91 2.14 1.9370 0 9 9 47.03 6.13 1.9323 0 14 1 47.03 3.26 1.9320 0 5 11 47.49 1.58 1.9145 -1 11 5 47.50 1.48 1.9142 1 11 5 47.57 1.15 1.9117 0 14 2 47.93 1.45 1.8979 0 13 5 48.13 2.62 1.8904 0 1 12 48.46 2.44 1.8784 -1 7 9 48.47 1.35 1.8779 1 7 9 49.03 3.49 1.8581 1 13 0 49.07 2.88 1.8566 0 12 7 49.12 3.00 1.8546 -1 10 7 49.13 2.22 1.8543 1 10 7 49.42 1.96 1.8440 1 9 8 49.43 3.87 1.8440 -1 11 6 49.43 3.98 1.8437 1 11 6 49.56 3.05 1.8392 -1 1 11 49.58 2.67 1.8387 1 1 11 49.85 4.02 1.8291 0 13 6 49.93 1.18 1.8266 -1 2 11 49.94 1.17 1.8261 1 2 11 50.18 1.09 1.8181 -1 6 10 50.29 1.57 1.8144 -1 8 9 50.58 2.08 1.8046 1 13 3 50.59 4.21 1.8043 0 15 1 50.64 7.95 1.8026 2 6 3 50.93 3.24 1.7932 -2 0 6 51.06 2.49 1.7887 2 1 6 51.21 1.26 1.7839 0 14 5 51.33 1.94 1.7799 -2 7 2 51.42 2.03 1.7772 2 2 6 51.63 1.51 1.7702 0 12 8 51.65 1.09 1.7696 1 11 7 51.69 1.41 1.7685 -1 10 8 51.78 6.77 1.7655 0 8 11 51.81 1.86 1.7645 -2 6 4 52.17 2.36 1.7533 -1 12 6 52.17 10.39 1.7533 -2 7 3 52.18 4.34 1.7531 1 12 6 52.18 7.13 1.7530 2 7 3 52.30 3.16 1.7492 -1 9 9 52.31 2.25 1.7488 1 9 9 52.42 1.72 1.7456 -1 5 11 52.43 2.17 1.7451 1 5 11 52.77 2.99 1.7349 0 2 13 53.04 6.72 1.7264 0 14 6 53.21 6.12 1.7214 -2 1 7 53.23 6.73 1.7208 2 1 7 53.32 2.71 1.7181 -1 0 12 53.33 6.78 1.7179 -2 7 4 53.34 2.99 1.7176 2 7 4 53.45 1.28 1.7143 1 1 12 53.73 1.46 1.7059 -1 14 3 53.74 1.07 1.7057 1 14 3 53.75 1.98 1.7053 0 9 11 53.78 1.84 1.7045 -1 2 12 53.79 3.18 1.7041 1 2 12 53.84 1.06 1.7026 0 7 12 54.04 1.04 1.6969 0 16 0 54.20 1.57 1.6922 0 16 1 54.87 2.10 1.6732 -1 14 4 54.87 1.02 1.6731 1 14 4 55.03 1.88 1.6687 2 9 2 55.04 2.03 1.6686 -2 8 4 55.04 1.58 1.6685 -1 13 6 55.05 3.81 1.6683 2 8 4 55.16 2.05 1.6651 0 14 7 55.53 1.19 1.6549 -2 0 8 56.31 1.18 1.6339 -1 14 5 57.00 1.57 1.6158 1 15 3 57.11 4.92 1.6128 0 2 14 57.53 4.00 1.6020 0 14 8 58.01 1.84 1.5898 0 16 5 62.04 2.77 1.4960 -2 6 9 62.06 1.13 1.4956 2 6 9 63.39 1.02 1.4673 -2 7 9 63.71 1.59 1.4608 -2 5 10 63.73 3.79 1.4603 2 5 10 64.01 3.54 1.4545 -2 13 1 64.82 1.87 1.4384 -1 17 4 64.82 1.77 1.4383 1 17 4 64.83 1.50 1.4381 -2 6 10 64.95 2.32 1.4358 2 8 9 66.76 1.38 1.4012 2 14 1 67.35 1.70 1.3904 -1 18 3 67.35 1.62 1.3903 1 18 3 67.53 1.18 1.3871 1 14 10 67.60 1.08 1.3858 0 19 4 68.21 1.03 1.3749 0 5 16 68.41 1.06 1.3714 2 12 7 68.58 1.08 1.3683 -1 12 12 69.05 1.25 1.3603 2 13 6 69.32 1.60 1.3556 -1 6 15 69.34 1.35 1.3553 1 6 15 69.68 2.19 1.3494 -1 9 14 69.70 1.98 1.3491 1 9 14 69.83 1.40 1.3469 -1 11 13 69.85 1.46 1.3466 1 11 13 70.62 1.55 1.3338 -2 8 11 70.64 1.06 1.3334 2 8 11 71.01 1.48 1.3274 1 19 3 71.68 1.24 1.3166 -2 14 6 71.70 1.83 1.3164 2 14 6 73.60 1.25 1.2870 -3 3 5 73.62 1.34 1.2867 3 3 5 75.15 1.15 1.2642 -2 2 14 75.18 1.17 1.2638 2 2 14 75.53 1.61 1.2589 -2 14 8 76.27 1.20 1.2485 -1 16 11 76.28 1.07 1.2483 1 16 11 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.