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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050271
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.032
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   17.2089 5.157962  -2  0  1    2   17.2105  5.157483    0.0016  0.000479
   18.3878 4.829268   2  0  0    2   18.3854  4.829888   -0.0024 -0.000620
   24.0563 3.701115   1  1  0    2   24.0596  3.700616    0.0033  0.000499
   25.5897 3.482429  -1  1  1    2   25.5899  3.482398    0.0002  0.000031
   29.8932 2.989629   1  1  1    2   29.8930  2.989646   -0.0002 -0.000018
   33.1399 2.703497  -4  0  1    2   33.1343  2.703945   -0.0056 -0.000447
   35.7736 2.510091   3  1  0    2   35.7783  2.509774    0.0047  0.000317
   36.7338 2.446595  -3  1  2    2   36.7368  2.446405    0.0030  0.000191
   41.6072 2.170376  -4  0  3    2   41.6062  2.170426   -0.0010 -0.000050
   44.9859 2.014787  -1  1  3    2   44.9752  2.015243   -0.0107 -0.000456
   45.7668 1.982186   4  0  1    2   45.7619  1.982385   -0.0049 -0.000200
   48.7562 1.867330  -2  2  1    2   48.7587  1.867239    0.0025  0.000091
   50.4560 1.808295  -6  0  2    2   50.4607  1.808137    0.0047  0.000158
   50.9656 1.791393  -2  0  4    2   50.9615  1.791528   -0.0041 -0.000136
   52.9356 1.729232   1  1  3    2   52.9422  1.729031    0.0066  0.000201
   55.7893 1.647299  -3  1  4    2   55.7973  1.647081    0.0080  0.000218
   63.1417 1.471922  -4  2  3    2   63.1369  1.472022   -0.0048 -0.000100
   65.7271 1.420115  -7  1  3    2   65.7262  1.420132   -0.0009 -0.000017

 rmse = 0.00005703623
 
     A =10.8616(6)             B =4.0063(3)               C =7.2356(4)           
 Alpha =90                  Beta =117.208(6)          Gamma =90                  
 
 Volume = 280.01(3)