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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070209
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.011
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   14.7587 6.001840   1  0  0    2   14.7555  6.003122   -0.0032 -0.001282
   15.1994 5.828667  -1  1  0    2   15.1974  5.829431   -0.0020 -0.000764
   18.4359 4.811444   1 -1  1    2   18.4335  4.812057   -0.0024 -0.000613
   21.4627 4.138898   0  1  1    2   21.4570  4.139977   -0.0057 -0.001079
   21.9606 4.046123  -1  0  2    2   21.9620  4.045871    0.0014  0.000252
   25.6232 3.475210   1  1  0    2   25.6273  3.474662    0.0041  0.000549
   26.5673 3.353765  -2  1  1    2   26.5642  3.354155   -0.0031 -0.000389
   30.0624 2.971188   2 -1  1    2   30.0600  2.971417   -0.0024 -0.000229
   30.3194 2.946576   1  0  2    2   30.3224  2.946291    0.0030  0.000285
   31.3575 2.851321  -1  0  3    2   31.3651  2.850649    0.0076  0.000672
   32.2772 2.772116   2 -2  1    2   32.2767  2.772154   -0.0005 -0.000039
   32.9465 2.717294  -2  2  1    2   32.9534  2.716744    0.0069  0.000551
   35.1022 2.555146   2  0  1    2   35.0999  2.555309   -0.0023 -0.000163
   36.5717 2.455746  -2  0  3    2   36.5609  2.456444   -0.0108 -0.000698
   37.3576 2.405854   2 -2  2    2   37.3548  2.406029   -0.0028 -0.000175
   37.6226 2.389510   1 -2  3    2   37.6215  2.389579   -0.0011 -0.000069
   38.2326 2.352765  -1  2  2    2   38.2351  2.352618    0.0025  0.000147
   38.7386 2.323181  -2  1  3    2   38.7411  2.323038    0.0025  0.000143
   40.0967 2.247547  -3  1  0    2   40.1026  2.247232    0.0059  0.000315
   44.2383 2.046209  -2  3  1    2   44.2395  2.046158    0.0012  0.000051
   44.5044 2.034587   0  0  4    2   44.5055  2.034538    0.0011  0.000049
   45.6039 1.988045   1  2  1    2   45.6047  1.988011    0.0008  0.000034
   48.5890 1.872626   3 -2  2    2   48.5867  1.872711   -0.0023 -0.000085
   50.0758 1.820441  -2  3  2    2   50.0709  1.820610   -0.0049 -0.000168
   51.2511 1.781411   0  3  1    2   51.2503  1.781436   -0.0008 -0.000025
   51.5508 1.771754   0 -3  4    2   51.5523  1.771706    0.0015  0.000049
   63.8248 1.457379  -4  4  0    2   63.8258  1.457358    0.0010  0.000021

 rmse = 0.00003678320
 
     A =6.9577(4)              B =6.9578(3)               C =8.8894(5)           
 Alpha =104.077(4)          Beta =101.209(5)          Gamma =113.914(4)          
 
 Volume = 360.15(3)