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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050132
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.049
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    8.8999 9.982362   0  0  2    2    8.9030  9.978905    0.0031  0.003458
   17.8125 4.988932   0  0  4    2   17.8106  4.989452   -0.0019 -0.000520
   19.9566 4.456193  -1  1  1    2   19.9624  4.454911    0.0058  0.001282
   22.4420 3.966908   1  1  2    2   22.4422  3.966869    0.0002  0.000039
   23.0060 3.870711  -1  1  3    2   23.0015  3.871457   -0.0045 -0.000747
   23.8885 3.729385   0  2  3    2   23.8916  3.728903    0.0031  0.000482
   25.5967 3.483769  -1  1  4    2   25.6001  3.483308    0.0034  0.000461
   27.8695 3.204111   1  1  4    2   27.8728  3.203744    0.0033  0.000368
   29.9440 2.986325   0  2  5    2   29.9380  2.986907   -0.0060 -0.000582
   31.2549 2.863800   1  1  5    2   31.2508  2.864168   -0.0041 -0.000368
   32.1568 2.785386  -1  1  6    2   32.1546  2.785573   -0.0022 -0.000187
   33.5111 2.675685   0  2  6    2   33.5142  2.675445    0.0031  0.000241
   45.4538 1.995822   0  0 10    2   45.4548  1.995781    0.0010  0.000041

 rmse = 0.00002762758
 
     A =5.1937(8)              B =9.005(2)                C =20.052(1)           
 Alpha =90                  Beta =95.555(8)           Gamma =90                  
 
 Volume = 933.5(2)