Pseudoboleite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from the powder pattern of R050162 Giuseppetti G, Mazzi F, Tadini C Neues Jahrbuch fur Mineralogie, Monatshefte 1992 (1992) 113-126 The crystal structure of pseudoboleite: Pb31Cu24Cl62(OH)48; its relations with the structures of boleite and cumengeite Locality: Boleo, Baja California, Mexico CELL PARAMETERS: 15.2410 15.2410 30.8280 90.000 90.000 90.000 SPACE GROUP: I4/mmm ATOM X Y Z OCCUPANCY ISO(B) Pb 0.00000 0.27500 0.24210 1.000 2.282 Pb 0.30420 0.30420 0.15100 1.000 2.061 Pb 0.00000 0.50000 0.13510 1.000 2.432 Pb 0.27400 0.50000 0.00000 1.000 2.629 Pb 0.00000 0.00000 0.39270 0.687 2.219 Pb 0.00000 0.00000 0.37060 0.313 2.479 Pb 0.15470 0.00000 0.00000 0.476 4.469 Pb 0.00000 0.00000 0.08370 0.468 5.630 Pb 0.00000 0.50000 0.00000 0.449 4.272 Pb 0.00000 0.00000 0.27160 0.631 4.161 Cu 0.25660 0.09530 0.12670 1.000 1.690 Cu 0.25650 0.25650 0.04710 1.000 1.753 Cl 0.37810 0.11610 0.30760 1.000 2.440 Cl 0.38370 0.38370 0.05920 1.000 2.550 Cl 0.37800 0.37800 0.43830 1.000 4.122 Cl 0.35790 0.35790 0.25120 1.000 3.237 Cl 0.00000 0.17360 0.34020 1.000 3.348 Cl 0.00000 0.37040 0.43410 1.000 2.329 Cl 0.32650 0.00000 0.00000 1.000 2.606 Cl 0.00000 0.00000 0.17390 1.000 3.040 OH 0.19120 0.31180 0.09430 1.000 2.400 OH 0.31080 0.31080 0.34600 1.000 1.445 OH 0.00000 0.33060 0.10510 1.000 1.966 OH 0.00000 0.21080 0.16320 1.000 1.840 OH 0.20990 0.32930 0.00000 1.000 2.163 X-RAY WAVELENGTH: 1.541838 BOUNDS ON TWO THETA: 0.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 13 +/- 13 +/- 28 MAX. ABS. INTENSITY / VOLUME**2: 60.12149162 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 5.73 7.25 15.4140 0 0 2 6.47 12.09 13.6625 1 0 1 10.01 4.56 8.8323 1 1 2 10.38 1.75 8.5203 1 0 3 11.48 1.02 7.7070 0 0 4 14.13 1.73 6.2689 1 1 4 15.50 1.10 5.7156 1 0 5 15.60 17.91 5.6801 2 1 3 16.36 2.93 5.4188 2 0 4 16.45 1.22 5.3885 2 2 0 17.26 2.52 5.1380 0 0 6 17.43 8.44 5.0866 2 2 2 17.69 2.68 5.0127 3 0 1 18.41 3.01 4.8196 3 1 0 19.14 1.24 4.6379 1 1 6 19.30 5.69 4.6000 3 1 2 19.41 5.08 4.5724 2 1 5 19.49 14.34 4.5542 3 0 3 20.11 100.00 4.4162 2 2 4 20.85 4.97 4.2601 2 0 6 21.00 2.86 4.2309 1 0 7 21.22 2.41 4.1879 3 2 1 21.75 5.35 4.0864 3 1 4 22.75 19.90 3.9093 3 2 3 23.08 26.00 3.8535 0 0 8 23.35 49.72 3.8103 4 0 0 23.93 5.28 3.7185 2 2 6 24.06 2.17 3.6990 2 1 7 24.78 4.16 3.5923 3 3 0 25.34 19.27 3.5152 3 1 6 25.46 13.13 3.4986 3 3 2 25.61 2.69 3.4783 4 1 3 25.91 2.06 3.4388 2 0 8 26.09 1.87 3.4156 4 0 4 26.15 3.03 3.4080 4 2 0 26.79 3.61 3.3277 3 0 7 26.79 5.06 3.3276 4 2 2 28.15 2.91 3.1704 4 1 5 28.48 10.12 3.1345 2 2 8 28.64 20.67 3.1169 4 2 4 28.96 6.67 3.0828 0 0 10 29.18 13.01 3.0606 2 1 9 29.45 16.04 3.0334 5 0 1 29.68 2.99 3.0097 3 1 8 30.36 13.24 2.9441 3 3 6 30.59 7.94 2.9223 5 0 3 30.59 1.98 2.9223 4 3 3 31.30 8.10 2.8578 2 0 10 31.50 1.48 2.8401 3 0 9 31.60 2.37 2.8313 4 1 7 31.75 3.25 2.8183 5 2 1 32.12 1.01 2.7868 5 1 4 32.82 4.41 2.7286 5 2 3 33.06 37.41 2.7094 4 0 8 33.25 21.06 2.6943 4 4 0 33.49 1.88 2.6758 2 2 10 33.77 2.48 2.6540 4 4 2 34.31 3.71 2.6138 5 3 0 34.54 9.44 2.5970 3 1 10 34.61 7.06 2.5920 2 1 11 34.72 8.39 2.5836 5 1 6 34.81 5.26 2.5770 5 3 2 34.93 2.11 2.5690 0 0 12 35.15 15.02 2.5529 4 2 8 35.29 8.56 2.5433 4 4 4 35.33 7.80 2.5402 6 0 0 35.74 2.56 2.5125 4 1 9 35.83 10.07 2.5064 5 0 7 35.83 1.38 2.5064 4 3 7 35.94 1.27 2.4990 1 1 12 36.29 5.83 2.4753 5 3 4 36.62 1.30 2.4539 3 0 11 36.93 8.82 2.4343 6 1 3 37.53 2.96 2.3966 4 0 10 37.70 1.58 2.3861 4 4 6 37.78 11.51 2.3809 5 2 7 37.79 5.22 2.3809 6 2 2 37.91 8.42 2.3732 5 4 1 38.10 2.82 2.3618 5 1 8 38.48 9.47 2.3395 3 3 10 38.54 6.19 2.3358 3 2 11 38.65 20.86 2.3297 5 3 6 38.83 8.49 2.3189 2 2 12 39.17 14.41 2.3000 6 2 4 39.58 2.82 2.2771 4 3 9 39.58 1.22 2.2771 6 0 6 40.27 1.13 2.2397 2 1 13 40.39 1.31 2.2333 4 1 11 40.87 1.11 2.2081 4 4 8 40.99 1.03 2.2020 0 0 14 41.38 7.13 2.1818 5 2 9 41.76 3.44 2.1631 5 3 8 42.05 3.66 2.1488 3 0 13 42.11 3.24 2.1459 5 1 10 42.34 1.68 2.1346 5 5 2 42.34 1.27 2.1346 7 1 2 42.44 1.96 2.1301 4 0 12 42.63 3.93 2.1208 6 0 8 42.78 3.66 2.1135 6 4 0 43.20 4.44 2.0940 5 4 7 43.60 3.73 2.0758 5 5 4 43.60 2.79 2.0758 7 1 4 43.77 1.02 2.0682 3 2 13 43.88 1.84 2.0631 5 0 11 44.15 2.30 2.0514 4 2 12 44.15 5.18 2.0514 7 2 3 44.33 1.26 2.0432 6 2 8 44.44 1.74 2.0384 2 2 14 44.45 1.80 2.0383 6 4 4 44.67 1.90 2.0287 4 4 10 44.89 2.59 2.0191 6 3 7 45.28 5.28 2.0029 3 1 14 45.50 6.73 1.9937 5 3 10 45.64 3.78 1.9876 5 5 6 45.64 6.98 1.9876 7 1 6 45.72 7.37 1.9846 7 3 2 46.13 1.43 1.9677 2 1 15 46.46 3.47 1.9546 5 4 9 47.17 2.15 1.9267 0 0 16 47.42 1.26 1.9171 6 5 3 47.74 6.62 1.9051 8 0 0 48.65 1.38 1.8717 5 0 13 48.65 1.24 1.8717 4 3 13 48.75 1.78 1.8680 2 0 16 48.75 3.37 1.8679 6 1 11 48.84 2.33 1.8648 7 3 6 48.99 1.01 1.8593 4 4 12 49.17 3.29 1.8531 6 4 8 49.27 2.79 1.8495 8 0 4 49.30 1.03 1.8483 3 2 15 49.30 2.30 1.8482 8 2 0 50.29 4.59 1.8143 2 2 16 50.53 5.23 1.8063 6 0 12 50.80 10.95 1.7973 8 2 4 50.83 3.13 1.7962 6 6 0 51.13 1.14 1.7863 7 2 9 51.14 1.99 1.7863 8 0 6 51.30 1.34 1.7808 8 3 1 52.03 11.01 1.7576 6 2 12 52.03 1.31 1.7575 8 3 3 52.20 2.03 1.7524 2 1 17 52.30 5.59 1.7493 6 6 4 52.63 1.11 1.7391 8 2 6 53.04 2.10 1.7267 7 5 4 53.67 1.21 1.7078 8 0 8 53.80 1.15 1.7041 4 3 15 53.80 1.24 1.7040 8 4 0 54.23 1.18 1.6914 1 1 18 54.49 2.39 1.6840 5 3 14 54.68 1.82 1.6786 7 3 10 54.73 2.07 1.6772 7 2 11 54.81 2.18 1.6749 7 5 6 54.87 2.27 1.6731 9 1 2 55.20 1.06 1.6639 6 0 14 55.24 1.81 1.6630 5 2 15 55.59 1.30 1.6533 8 3 7 56.85 1.93 1.6194 5 1 16 57.09 1.24 1.6134 1 0 19 57.46 1.79 1.6038 7 0 13 57.77 1.26 1.5959 8 5 3 58.47 1.47 1.5784 2 1 19 58.93 1.03 1.5672 4 4 16 59.30 3.23 1.5584 8 4 8 60.02 1.21 1.5414 0 0 20 60.07 1.61 1.5403 5 5 14 60.07 2.20 1.5403 7 1 14 60.25 2.65 1.5361 7 5 10 60.43 1.85 1.5320 7 7 2 60.65 3.07 1.5269 5 2 17 60.77 3.63 1.5241 10 0 0 61.36 1.07 1.5108 2 0 20 61.54 1.54 1.5068 6 5 13 62.37 2.64 1.4888 9 2 9 62.52 1.27 1.4857 4 1 19 62.74 1.17 1.4810 7 3 14 62.87 1.27 1.4782 7 4 13 62.91 1.11 1.4773 9 1 10 63.03 1.22 1.4748 7 7 6 63.16 1.41 1.4721 6 6 12 63.42 1.42 1.4666 7 2 15 63.69 2.72 1.4612 8 5 9 64.91 1.16 1.4365 5 5 16 65.12 1.37 1.4325 5 3 18 65.52 1.34 1.4247 9 3 10 65.63 1.13 1.4225 9 5 6 65.76 1.22 1.4200 8 7 3 65.91 1.41 1.4173 10 0 8 65.99 1.89 1.4157 8 2 14 66.02 1.20 1.4151 6 5 15 66.02 1.74 1.4151 10 4 0 66.33 1.04 1.4092 10 4 2 66.59 1.75 1.4044 4 2 20 67.18 1.02 1.3934 10 2 8 67.90 1.61 1.3804 7 5 14 68.07 1.04 1.3774 7 7 10 69.37 4.79 1.3547 8 0 16 69.82 2.79 1.3471 8 8 0 70.19 1.07 1.3409 5 5 18 70.37 1.25 1.3379 4 4 20 70.58 2.68 1.3345 9 5 10 70.95 4.49 1.3284 10 4 8 72.39 1.05 1.3055 3 3 22 72.84 1.29 1.2985 6 2 20 73.16 4.87 1.2937 11 3 6 73.28 1.34 1.2918 10 2 12 73.50 1.49 1.2885 10 6 4 74.23 1.28 1.2777 3 2 23 77.13 2.16 1.2366 12 2 4 79.45 1.72 1.2063 8 5 17 79.45 1.09 1.2063 12 0 8 79.56 1.14 1.2049 12 4 0 79.91 1.25 1.2004 9 1 18 81.43 1.08 1.1818 10 5 13 84.86 1.72 1.1427 11 3 14 85.12 1.74 1.1398 11 7 6 88.50 1.25 1.1048 6 5 23 89.71 1.23 1.0930 13 1 10 89.87 1.36 1.0915 13 5 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.