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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070130
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.017
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   19.0448 4.660201   1  1  1    2   19.0433  4.660556   -0.0015 -0.000355
   20.2872 4.377289   2  0  0    2   20.2903  4.376636    0.0031  0.000653
   23.4637 3.790964   2  0  2    2   23.4618  3.791267   -0.0019 -0.000303
   25.8525 3.445609  -2  0  4    2   25.8489  3.446077   -0.0036 -0.000469
   29.5084 3.026268   2  0  4    2   29.5071  3.026395   -0.0013 -0.000128
   32.7190 2.736119  -2  0  6    2   32.7187  2.736139   -0.0003 -0.000021
   34.0324 2.633417  -3  1  1    2   34.0334  2.633339    0.0010  0.000078
   35.8051 2.506935   0  2  4    2   35.8000  2.507278   -0.0051 -0.000343
   39.4843 2.281298  -3  1  5    2   39.4908  2.280934    0.0065  0.000363
   40.8633 2.207406  -2  0  8    2   40.8590  2.207630   -0.0043 -0.000223
   41.8329 2.158437   0  2  6    2   41.8368  2.158246    0.0039  0.000190
   42.7522 2.114110   2  2  4    2   42.7547  2.113993    0.0025  0.000116
   43.2092 2.092794  -4  0  4    2   43.2108  2.092720    0.0016  0.000074
   47.3412 1.919253  -4  0  6    2   47.3396  1.919313   -0.0016 -0.000060
   57.7564 1.595374   4  2  4    2   57.7545  1.595422   -0.0019 -0.000048
   58.3563 1.580390   0  0 12    2   58.3577  1.580355    0.0014  0.000035
   59.4094 1.554857  -2  2 10    2   59.4085  1.554878   -0.0009 -0.000021

 rmse = 0.00003044176
 
     A =8.8277(4)              B =5.9084(4)               C =19.1254(6)          
 Alpha =90                  Beta =97.444(4)           Gamma =90                  
 
 Volume = 989.12(6)