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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 Rasvumite__R060491-9__Powder__Xray_Data_XY_Processed__10240[1]
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  0.710710
 Wavelength #2 =  0.709270
 Wavelength #3 =  0.713590
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.037
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    5.8234 7.026124   1  1  0    2    5.8266  7.022215    0.0032  0.003909
    7.3594 5.553678   0  2  0    2    7.3772  5.540253    0.0178  0.013425
   20.5472 1.991990   3  1  2    2   20.5497  1.991745    0.0025  0.000245
   21.0681 1.943187   0  4  2    2   21.0764  1.942430    0.0083  0.000757
   22.1729 1.847323   0  6  0    2   22.1798  1.846751    0.0069  0.000572
   24.2960 1.687763   1  5  2    2   24.2756  1.689159   -0.0204 -0.001396
   30.2429 1.361083   0  0  4    2   30.2168  1.362232   -0.0261 -0.001149
   31.1105 1.323977   0  2  4    2   31.1381  1.322832    0.0276  0.001145

 rmse = 0.00067040687
 
     A =9.08(3)                B =11.08(1)                C =5.449(2)            
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 540(2)