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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060106
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.027
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   24.6507 3.612453  -2  2  1    2   24.6624  3.610762    0.0117  0.001691
   31.2314 2.863991   0  2  2    2   31.2383  2.863370    0.0069  0.000621
   36.3005 2.474536  -1  5  1    2   36.3069  2.474115    0.0064  0.000421
   36.7870 2.442895   3  0  1    2   36.7914  2.442614    0.0044  0.000281
   29.0252 3.076673   0  1  2    2   29.0285  3.076325    0.0033  0.000347
   15.4843 5.727911   0  1  1    2   15.4875  5.726740    0.0032  0.001171
   50.2024 1.816691  -3  6  1    2   50.2046  1.816616    0.0022  0.000076
   30.5564 2.925759   2  2  1    2   30.5586  2.925555    0.0022  0.000204
   33.7628 2.654649  -2  4  1    2   33.7637  2.654584    0.0009  0.000065
   13.0684 6.783091   0  2  0    2   13.0688  6.782879    0.0004  0.000212
   39.8647 2.260971   0  6  0    2   39.8649  2.260960    0.0002  0.000012
   29.2712 3.051349  -3  0  1    2   29.2710  3.051372   -0.0002 -0.000024
   14.7106 6.027943  -1  0  1    2   14.7098  6.028270   -0.0008 -0.000327
   40.4731 2.228353  -3  3  2    2   40.4721  2.228404   -0.0010 -0.000050
   16.4151 5.404609   1  2  0    2   16.4138  5.405043   -0.0013 -0.000435
   23.8371 3.734020   2  2  0    2   23.8355  3.734269   -0.0016 -0.000249
   11.8692 7.467171   1  1  0    2   11.8670  7.468538   -0.0022 -0.001367
   38.1361 2.359458  -1  4  2    2   38.1330  2.359644   -0.0031 -0.000186
   21.8557 4.068280  -2  1  1    2   21.8520  4.068959   -0.0037 -0.000678
   23.4335 3.797486   1  2  1    2   23.4297  3.798089   -0.0038 -0.000603
   32.1706 2.782418  -3  2  1    2   32.1666  2.782754   -0.0040 -0.000335
   16.1074 5.507330  -1  1  1    2   16.1029  5.508847   -0.0045 -0.001517
   36.0796 2.489190   3  3  0    2   36.0748  2.489513   -0.0048 -0.000323
   47.0940 1.929164   1  5  2    2   47.0890  1.929359   -0.0050 -0.000195
   19.2164 4.621472   0  2  1    2   19.2108  4.622815   -0.0056 -0.001343
   24.2192 3.675901   0  3  1    2   24.2119  3.676988   -0.0073 -0.001087

 rmse = 0.00003358262
 
     A =9.3293(6)              B =13.5658(7)              C =6.5876(6)           
 Alpha =90                  Beta =106.472(6)          Gamma =90                  
 
 Volume = 799.50(7)