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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060363
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.008
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   12.4696 7.097095   1  1  0    2   12.4630  7.100849   -0.0066 -0.003754
   13.3316 6.639811  -1  1  0    2   13.3325  6.639367    0.0009  0.000444
   18.6718 4.750301   2  0  0    2   18.6744  4.749651    0.0026  0.000650
   25.0683 3.550431   2  2  0    2   25.0683  3.550425    0.0000  0.000006
   30.1674 2.960759   2 -2  2    2   30.1674  2.960756    0.0000  0.000003
   30.5197 2.927371   1  1  3    2   30.5198  2.927366    0.0001  0.000006
   32.4254 2.759501  -2 -2  4    2   32.4254  2.759504    0.0000 -0.000004
   34.5675 2.593204   0 -4  1    2   34.5683  2.593147    0.0008  0.000057
   35.8067 2.506228  -3 -3  1    2   35.8065  2.506239   -0.0002 -0.000011
   41.5072 2.174182   2 -4  1    2   41.5067  2.174207   -0.0005 -0.000024

 rmse = 0.00001289125
 
     A =     9.7672(9)       B =    10.5146(5)        C =    12.2421(7)    
 Alpha =   109.111(9)     Beta =   102.897(7)     Gamma =    82.245(4)     
 
 Volume =   1155.37(9)