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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060549
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.033
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   12.4688 7.112082   1  1  0    2   12.4670  7.113095   -0.0018 -0.001013
   13.3158 6.660395  -1  1  0    2   13.3230  6.656789    0.0072  0.003606
   18.6605 4.759618   2  0  0    2   18.6542  4.761210   -0.0063 -0.001591
   21.5934 4.118314   0  2  1    2   21.5937  4.118249    0.0003  0.000065
   25.0497 3.556598   2  2  0    2   25.0501  3.556547    0.0004  0.000051
   28.4966 3.133242   1 -3  1    2   28.5019  3.132669    0.0053  0.000573
   30.5269 2.929092   1  1  3    2   30.5240  2.929362   -0.0029 -0.000269
   32.4615 2.758628  -2 -2  4    2   32.4618  2.758601    0.0003  0.000027
   33.8233 2.650499   0  2  3    2   33.8236  2.650473    0.0003  0.000026
   34.5894 2.593471   0 -4  1    2   34.5867  2.593664   -0.0027 -0.000193
   35.7741 2.510173  -3 -3  1    2   35.7746  2.510137    0.0005  0.000036
   40.6212 2.220884   2  2  3    2   40.6225  2.220816    0.0013  0.000068
   41.5055 2.175549   2 -4  1    2   41.5048  2.175583   -0.0007 -0.000034

 rmse = 0.00002414543
 
     A =9.802(2)               B =10.5076(9)              C =12.223(1)           
 Alpha =108.68(1)           Beta =103.19(1)           Gamma =82.287(7)           
 
 Volume = 1158.6(1)