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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R061053
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.024
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   10.2931 8.607103   2  0  0    2   10.2935  8.606775    0.0004  0.000327
   17.9050 4.956526   3  1  0    2   17.9084  4.955596    0.0034  0.000930
   26.2773 3.391768   3  1  2    2   26.2767  3.391847   -0.0006 -0.000079
   28.3773 3.145146   2  2  2    2   28.3763  3.145256   -0.0010 -0.000110
   29.3573 3.042260   1  3  1    2   29.3565  3.042342   -0.0008 -0.000081
   36.2470 2.477855   6  2  0    2   36.2479  2.477798    0.0009  0.000057
   36.5532 2.457785   0  4  0    2   36.5525  2.457833   -0.0007 -0.000048
   38.7004 2.326132   0  0  4    2   38.6997  2.326173   -0.0007 -0.000040
   41.2691 2.187001   6  2  2    2   41.2698  2.186966    0.0007  0.000035
   42.9085 2.107114   2  4  2    2   42.9094  2.107070    0.0009  0.000044
   50.6662 1.801028   3  3  4    2   50.6666  1.801014    0.0004  0.000014
   53.6594 1.707364   5  5  0    2   53.6578  1.707410   -0.0016 -0.000046
   54.0528 1.695857   6  2  4    2   54.0505  1.695924   -0.0023 -0.000066
   54.2713 1.689542   0  4  4    2   54.2734  1.689481    0.0021  0.000061
   59.3406 1.556673   9  3  2    2   59.3414  1.556655    0.0008  0.000018

 rmse = 0.00001425732
 
     A =17.2136(4)             B =9.8313(2)               C =9.3047(2)           
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 1574.65(4)