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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060673
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.091
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   14.4384 6.168246   2  1  0    2   14.4439  6.165892    0.0055  0.002354
   16.5387 5.385016   2  2  0    2   16.5309  5.387553   -0.0078 -0.002537
   21.9611 4.060592   1  0  6    2   21.9586  4.061052   -0.0025 -0.000460
   23.1154 3.859564   2  4  0    2   23.1010  3.861946   -0.0144 -0.002382
   23.8561 3.740921   1  2  6    2   23.8635  3.739780    0.0074  0.001141
   26.0600 3.428224   1  3  6    2   26.0593  3.428319   -0.0007 -0.000095
   27.0405 3.305680   2  5  0    2   27.0380  3.305982   -0.0025 -0.000302
   27.4627 3.255642   4  0  0    2   27.4628  3.255631    0.0001  0.000011
   27.8545 3.210582   4  1  0    2   27.8618  3.209753    0.0073  0.000829
   29.3877 3.045955   3  0  6    2   29.3912  3.045603    0.0035  0.000352
   29.7666 3.007921   3  1  6    2   29.7664  3.007945   -0.0002 -0.000023
   30.8605 2.903433   3  2  6    2   30.8670  2.902835    0.0065  0.000598
   31.2256 2.870213   2  6  0    2   31.2240  2.870352   -0.0016 -0.000139
   32.6201 2.750283   3  3  6    2   32.6266  2.749748    0.0065  0.000535
   39.7411 2.271211   1  7  6    2   39.7280  2.271932   -0.0131 -0.000720
   42.3531 2.136684   0  0 12    2   42.3445  2.137099   -0.0086 -0.000415
   43.8833 2.065506   1  8  6    2   43.8918  2.065125    0.0085  0.000381
   44.9694 2.018009   5  4  6    2   44.9751  2.017764    0.0057  0.000245
   45.9524 1.977016   6  4  0    2   45.9426  1.977417   -0.0098 -0.000401
   46.8491 1.941169   5  4  7    2   46.8492  1.941166    0.0001  0.000003
   47.4243 1.918913   0 10  0    2   47.4298  1.918704    0.0055  0.000209
   48.3538 1.884105   3  8  6    2   48.3495  1.884264   -0.0043 -0.000159
   49.9911 1.826052   5  6  6    2   49.9952  1.825912    0.0041  0.000141
   50.9176 1.794919   2  5 12    2   50.9225  1.794756    0.0049  0.000163
   55.6412 1.652954   4 10  0    2   55.6398  1.652991   -0.0014 -0.000037
   64.1975 1.451422   6  4 12    2   64.1977  1.451417    0.0002  0.000005
   65.3941 1.427691   0 10 12    2   65.3928  1.427717   -0.0013 -0.000025

 rmse = 0.00005581355
 
     A =13.0225(9)             B =19.187(1)               C =25.645(2)           
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 6407.8(0)