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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070633
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.028
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   24.6302 3.615512   0 -2  2    2   24.6314  3.615343    0.0012  0.000169
   30.9611 2.888458   3 -3  1    2   30.9563  2.888898   -0.0048 -0.000440
   33.3736 2.684789   3 -1  1    2   33.3748  2.684699    0.0012  0.000091
   34.1830 2.622995  -3  2  2    2   34.1884  2.622593    0.0054  0.000402
   37.2949 2.410802   0 -3  3    2   37.3041  2.410229    0.0092  0.000573
   44.3990 2.039905  -2  0  4    2   44.3903  2.040287   -0.0087 -0.000382
   44.5231 2.034504   2 -5  1    2   44.5203  2.034625   -0.0028 -0.000121
   44.8028 2.022442   4 -1  1    2   44.8028  2.022440    0.0000  0.000002
   45.7781 1.981570  -5  3  1    2   45.7766  1.981633   -0.0015 -0.000062
   47.2520 1.923103  -2  1  4    2   47.2538  1.923034    0.0018  0.000069
   47.3737 1.918443  -2  5  0    2   47.3715  1.918528   -0.0022 -0.000085
   48.6495 1.871044  -4  4  2    2   48.6507  1.871001    0.0012  0.000043
   52.5806 1.739961   5 -4  2    2   52.5814  1.739938    0.0008  0.000023
   64.9403 1.435341  -4  5  3    2   64.9417  1.435313    0.0014  0.000028

 rmse = 0.00005106308
 
     A =10.0181(8)             B =10.4009(8)              C =8.6435(8)           
 Alpha =106.472(6)          Beta =95.98(1)            Gamma =124.39(1)           
 
 Volume = 671.8(1)