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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R040051
 
 Symmetry constraint is: HEXAGONAL   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.024
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   25.0614 3.553646   0  1  2    2   25.0560  3.554395   -0.0054 -0.000749
   32.5459 2.750884   1  0  4    2   32.5399  2.751375   -0.0060 -0.000492
   38.6692 2.327932   1  1  0    2   38.6678  2.328015   -0.0014 -0.000083
   42.8063 2.111906   1  1  3    2   42.8078  2.111834    0.0015  0.000072
   46.6302 1.947146   2  0  2    2   46.6218  1.947477   -0.0084 -0.000331
   51.3945 1.777188   0  2  4    2   51.3942  1.777198   -0.0003 -0.000009
   61.0815 1.516390   2  1  1    2   61.0858  1.516294    0.0043  0.000096
   62.1055 1.493814   1  2  2    2   62.1091  1.493735    0.0036  0.000079
   68.1191 1.375795   2  0  8    2   68.1252  1.375688    0.0061  0.000108
   69.1066 1.358521   1  1  9    2   69.1112  1.358441    0.0046  0.000080
   69.9542 1.344114   3  0  0    2   69.9562  1.344080    0.0020  0.000034
   81.1747 1.184233   1  2  8    2   81.1644  1.184357   -0.0103 -0.000124

 rmse = 0.00007135367
 
     A =     4.6560(2)         B =     4.6560(2)          C =    15.054(1)       
 Alpha =    90.             Beta =    90.             Gamma =   120.             
 
 Volume =    282.64(2)