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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060407

 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.073
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   27.3832 3.262875   1  1  5    2   27.4014  3.260748    0.0182  0.002127
   31.9435 2.805628   0  4  0    2   31.9523  2.804874    0.0088  0.000755
   26.6691 3.348841   2  2  0    2   26.6750  3.348116    0.0059  0.000725
   48.8921 1.863941   2  4  6    2   48.8946  1.863851    0.0025  0.000091
   45.8346 1.981109   1  1  9    2   45.8327  1.981186   -0.0019 -0.000076
   19.5348 4.557377   1  1  3    2   19.5316  4.558108   -0.0032 -0.000732
   32.9714 2.720277   0  2  6    2   32.9664  2.720682   -0.0050 -0.000405
   39.9595 2.258313   2  4  2    2   39.9530  2.258665   -0.0065 -0.000352
   29.9145 2.991611   1  3  3    2   29.9077  2.992273   -0.0068 -0.000662
   18.5184 4.806151   0  2  2    2   18.5109  4.808082   -0.0075 -0.001931
   14.1293 6.295485   1  1  1    2   14.1126  6.302942   -0.0167 -0.007457

 rmse = 0.00006631490
 
     A =8.346(4)               B =11.219(2)               C =18.666(2)           
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 1747.8(0)